(1R,2S,3S,4R,5R)-1-azido-2,3,4-tris(benzyloxy)-5-[(benzyloxy)methyl]cyclohexane

Base Information

Chemical Name:(1R,2S,3S,4R,5R)-1-azido-2,3,4-tris(benzyloxy)-5-[(benzyloxy)methyl]cyclohexane
CAS No.:184047-97-0
Molecular Formula:C₃₅H₃₇N₃O₄
Molecular Weight:563.696
Hs Code.:

Synonyms:(1R,2S,3S,4R,5R)-1-azido-2,3,4-tris(benzyloxy)-5-[(benzyloxy)methyl]cyclohexane

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Chemical Property of (1R,2S,3S,4R,5R)-1-azido-2,3,4-tris(benzyloxy)-5-[(benzyloxy)methyl]cyclohexane

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Technology Process of (1R,2S,3S,4R,5R)-1-azido-2,3,4-tris(benzyloxy)-5-[(benzyloxy)methyl]cyclohexane

There total 2 articles about (1R,2S,3S,4R,5R)-1-azido-2,3,4-tris(benzyloxy)-5-[(benzyloxy)methyl]cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: (1S,2S,3S,4R,5R)-2,3,4-tris(benzyloxy)-5-[(benzyloxy)methyl]cyclohexane-1-methanesulfonate

: 184047-97-0
(1R,2S,3S,4R,5R)-1-azido-2,3,4-tris(benzyloxy)-5-[(benzyloxy)methyl]cyclohexane

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 120 ℃; for 3h;
DOI:10.1002/hlca.200390178

Reference yield:

: 162119-25-7
(1S,2S,3S,4R,5R)-2,3,4-tris(benzyloxy)-5-[(benzyloxy)methyl]cyclohexanol

: 184047-97-0
(1R,2S,3S,4R,5R)-1-azido-2,3,4-tris(benzyloxy)-5-[(benzyloxy)methyl]cyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / pyridine

2: 94 percent / NaN₃ / dimethylformamide / 3 h / 120 °C

With pyridine; sodium azide; In N,N-dimethyl-formamide;
DOI:10.1002/hlca.200390178

Reference yield: 100.0%

: 184047-97-0
(1R,2S,3S,4R,5R)-1-azido-2,3,4-tris(benzyloxy)-5-[(benzyloxy)methyl]cyclohexane

: (1R,2S,3S,4R,6R)-4-amino-6-(hydroxymethyl)cyclohexane-1,2,3-triol

Guidance literature:: With hydrogenchloride; water; hydrogen; palladium on activated charcoal; In methanol; for 15h; under 4500.36 Torr;
DOI:10.1002/hlca.200390178