3-(((2S,3S,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol

Base Information

• Chemical Name: 3-(((2S,3S,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol
• CAS No.: 288590-07-8
• Molecular Formula: C₃₇H₄₂O₇
• Molecular Weight: 598.736

Synonyms:3-(((2S,3S,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol

Chemical Property of 3-(((2S,3S,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol

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Technology Process of 3-(((2S,3S,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol

There total 3 articles about 3-(((2S,3S,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

(3S,4S,5R,6R)-2-(allyloxy)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-tetrahydro-2H-pyran (194594-76-8) → 3-(((2S,3S,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol (288590-07-8)

Guidance literature:

(3S,4S,5R,6R)-2-(allyloxy)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-tetrahydro-2H-pyran; With 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; at 20 ℃; for 20h;

With sodium hydroxide; water; dihydrogen peroxide; at 20 ℃; for 48h; Further stages.;

DOI:10.1002/1099-0690(200006)2000:11<2027::AID-EJOC2027>3.0.CO;2-L

Reference yield: 86.0%

C48H57NO7 → C13H20N2O + 3-(diethylamino)benzaldehyde (116496-09-4) + (3-(diethylamino)phenyl)methanol (58293-93-9) + 3-(((2S,3S,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol (288590-07-8)

Guidance literature:

With water; acetonitrile; for 1.5h; UV-irradiation;

DOI:10.1021/acs.orglett.5b00699

Reference yield: 82.0%

C58H61NO7 (1310450-13-5) → 3-(((2S,3S,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol (288590-07-8)

Guidance literature:

In methanol; acetonitrile; at 20 - 30 ℃; for 4.5h; Irradiation;

DOI:10.1021/jo200692c

upstream raw materials:

(3S,4S,5R,6R)-2-(allyloxy)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-tetrahydro-2H-pyran

C₅₈H₆₁NO₇

Downstream raw materials:

C₅₈H₆₁NO₇

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