methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-β-D-arabino-hexapyranosyl)-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-β-D-arabino-hexapyranosyl)-α-D-glucopyranoside
CAS No.:125084-95-9
Molecular Formula:C₄₀H₄₈O₁₃
Molecular Weight:736.813
Hs Code.:

Synonyms:methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-β-D-arabino-hexapyranosyl)-α-D-glucopyranoside

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Chemical Property of methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-β-D-arabino-hexapyranosyl)-α-D-glucopyranoside

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Technology Process of methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-β-D-arabino-hexapyranosyl)-α-D-glucopyranoside

There total 14 articles about methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-β-D-arabino-hexapyranosyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 125084-94-8
methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-isocyano-β-D-glucopyranosyl)-α-D-glucopyranoside

: 125084-95-9
methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-β-D-arabino-hexapyranosyl)-α-D-glucopyranoside

Guidance literature:: With azobisisobutyronitrile; tri-n-butyl-tin hydride; In toluene; for 0.166667h; Heating;
DOI:10.1016/0008-6215(89)85044-X

Reference yield:

: 19488-48-3
methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: C₁₆H₂₂O₇S

: 145852-20-6
methyl O-(3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: 125084-95-9
methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-β-D-arabino-hexapyranosyl)-α-D-glucopyranoside

Guidance literature:: With [tris(para(trifluoromethyl)phenyl)phosphine]gold(I) chloride; silver trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 0.5h; Overall yield = 69 %; Molecular sieve;
DOI:10.1021/cs300670k

Reference yield:

: 19488-48-3
methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: C₂₁H₂₈O₉

: 145852-20-6
methyl O-(3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: 125084-95-9
methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-β-D-arabino-hexapyranosyl)-α-D-glucopyranoside

Guidance literature:: methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside; C₂₁H₂₈O₉; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere; Molecular sieve;

With triphenylphosphinegold(I) triflate; In dichloromethane; at 20 ℃; for 3h; Overall yield = 77 percent; Overall yield = 57 mg; Inert atmosphere; Molecular sieve;
DOI:10.1021/acs.orglett.9b03851