allyl 2-(anilinocarbonyl)-3-hydroxy-3-methyl-2,3,4,4a,5,6,7,8-octahydrocinnoline-4-carboxylate

Base Information

Chemical Name:allyl 2-(anilinocarbonyl)-3-hydroxy-3-methyl-2,3,4,4a,5,6,7,8-octahydrocinnoline-4-carboxylate
CAS No.:1242030-34-7
Molecular Formula:C₂₀H₂₅N₃O₄
Molecular Weight:371.436
Hs Code.:

Synonyms:allyl 2-(anilinocarbonyl)-3-hydroxy-3-methyl-2,3,4,4a,5,6,7,8-octahydrocinnoline-4-carboxylate

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Chemical Property of allyl 2-(anilinocarbonyl)-3-hydroxy-3-methyl-2,3,4,4a,5,6,7,8-octahydrocinnoline-4-carboxylate

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Technology Process of allyl 2-(anilinocarbonyl)-3-hydroxy-3-methyl-2,3,4,4a,5,6,7,8-octahydrocinnoline-4-carboxylate

There total 2 articles about allyl 2-(anilinocarbonyl)-3-hydroxy-3-methyl-2,3,4,4a,5,6,7,8-octahydrocinnoline-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1118-84-9
allyl acetoacetate

: 1025066-08-3
N-phenyl-2-(1-cyclohexenyl)-1-diazene-1-carboxamide

: 1242030-34-7
allyl 2-(anilinocarbonyl)-3-hydroxy-3-methyl-2,3,4,4a,5,6,7,8-octahydrocinnoline-4-carboxylate

: C₂₀H₂₅N₃O₄

Guidance literature:: With sodium methylate; In tetrahydrofuran; at 20 ℃; regioselective reaction;
DOI:10.1016/j.tet.2010.06.061

Reference yield: 52.0%

: 1118-84-9
allyl acetoacetate

: 1025066-08-3
N-phenyl-2-(1-cyclohexenyl)-1-diazene-1-carboxamide

: 1242030-34-7
allyl 2-(anilinocarbonyl)-3-hydroxy-3-methyl-2,3,4,4a,5,6,7,8-octahydrocinnoline-4-carboxylate

: 1242030-50-7
allyl 1-[(anilinocarbonyl)amino]-2-methyl-4,5,6,7-tetrahydro-1H-indole-3-carboxylate

Guidance literature:: allyl acetoacetate; N-phenyl-2-(1-cyclohexenyl)-1-diazene-1-carboxamide; With sodium methylate; In tetrahydrofuran; at 20 ℃; for 0.5h;

With silica gel; In cyclohexane; ethyl acetate;
DOI:10.1016/j.tet.2010.06.061