cyclopentyl N₂-[(benzyloxy)carbonyl]-N₆-{5-[4-chloro-3-(methylsulfonyl)phenyl]-4-methyl-1,3-thiazol-2-yl}-6-oxo-L-lysinate

Base Information

• Chemical Name: cyclopentyl N₂-[(benzyloxy)carbonyl]-N₆-{5-[4-chloro-3-(methylsulfonyl)phenyl]-4-methyl-1,3-thiazol-2-yl}-6-oxo-L-lysinate
• CAS No.: 957185-16-9
• Molecular Formula: C₃₀H₃₄ClN₃O₇S₂
• Molecular Weight: 648.201

Synonyms:cyclopentyl N₂-[(benzyloxy)carbonyl]-N₆-{5-[4-chloro-3-(methylsulfonyl)phenyl]-4-methyl-1,3-thiazol-2-yl}-6-oxo-L-lysinate

Chemical Property of cyclopentyl N₂-[(benzyloxy)carbonyl]-N₆-{5-[4-chloro-3-(methylsulfonyl)phenyl]-4-methyl-1,3-thiazol-2-yl}-6-oxo-L-lysinate

Chemical Property:

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Technology Process of cyclopentyl N₂-[(benzyloxy)carbonyl]-N₆-{5-[4-chloro-3-(methylsulfonyl)phenyl]-4-methyl-1,3-thiazol-2-yl}-6-oxo-L-lysinate

There total 1 articles about cyclopentyl N₂-[(benzyloxy)carbonyl]-N₆-{5-[4-chloro-3-(methylsulfonyl)phenyl]-4-methyl-1,3-thiazol-2-yl}-6-oxo-L-lysinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

5-[4-chloro-3-(methylsulfonyl)phenyl]-4-methyl-1,3-thiazol-2-amine (593959-38-7) + cyclopentyl N-[(benzyloxy)carbonyl]-6-hydroxy-6-oxo-L-norleucinate (957185-04-5) → cyclopentyl N2-[(benzyloxy)carbonyl]-N6-{5-[4-chloro-3-(methylsulfonyl)phenyl]-4-methyl-1,3-thiazol-2-yl}-6-oxo-L-lysinate (957185-16-9)

Guidance literature:

cyclopentyl N-[(benzyloxy)carbonyl]-6-hydroxy-6-oxo-L-norleucinate; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;

5-[4-chloro-3-(methylsulfonyl)phenyl]-4-methyl-1,3-thiazol-2-amine; With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 48h;

Reference yield: 74.0%

cyclopentyl N2-[(benzyloxy)carbonyl]-N6-{5-[4-chloro-3-(methylsulfonyl)phenyl]-4-methyl-1,3-thiazol-2-yl}-6-oxo-L-lysinate (957185-16-9) → cyclopentyl N6-{5-[4-chloro-3-(methylsulfonyl)phenyl]-4-methyl-1,3-thiazol-2-yl}-6-oxo-L-lysinate bis trifluoroacetate

Guidance literature:

With hydrogen bromide; In acetic acid; at 20 ℃; for 1.5h;

upstream raw materials:

5-[4-chloro-3-(methylsulfonyl)phenyl]-4-methyl-1,3-thiazol-2-amine

cyclopentyl N-[(benzyloxy)carbonyl]-6-hydroxy-6-oxo-L-norleucinate

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