N-[(2E,4E)-(1S,6S,7S)-1-((S)-1-[1,3]Dithian-2-yl-ethyl)-7-methoxy-4,6-dimethyl-8-phenyl-octa-2,4-dienyl]-2,2,2-trifluoro-acetamide

Base Information

Chemical Name:N-[(2E,4E)-(1S,6S,7S)-1-((S)-1-[1,3]Dithian-2-yl-ethyl)-7-methoxy-4,6-dimethyl-8-phenyl-octa-2,4-dienyl]-2,2,2-trifluoro-acetamide
CAS No.:182222-83-9
Molecular Formula:C₂₅H₃₄F₃NO₂S₂
Molecular Weight:501.678
Hs Code.:

Synonyms:N-[(2E,4E)-(1S,6S,7S)-1-((S)-1-[1,3]Dithian-2-yl-ethyl)-7-methoxy-4,6-dimethyl-8-phenyl-octa-2,4-dienyl]-2,2,2-trifluoro-acetamide

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Chemical Property of N-[(2E,4E)-(1S,6S,7S)-1-((S)-1-[1,3]Dithian-2-yl-ethyl)-7-methoxy-4,6-dimethyl-8-phenyl-octa-2,4-dienyl]-2,2,2-trifluoro-acetamide

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Technology Process of N-[(2E,4E)-(1S,6S,7S)-1-((S)-1-[1,3]Dithian-2-yl-ethyl)-7-methoxy-4,6-dimethyl-8-phenyl-octa-2,4-dienyl]-2,2,2-trifluoro-acetamide

There total 6 articles about N-[(2E,4E)-(1S,6S,7S)-1-((S)-1-[1,3]Dithian-2-yl-ethyl)-7-methoxy-4,6-dimethyl-8-phenyl-octa-2,4-dienyl]-2,2,2-trifluoro-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 182222-81-7
Methanesulfonic acid (E)-(1S,2R,5S,6S)-1-[(1R,2S)-2-[1,3]dithian-2-yl-1-(2,2,2-trifluoro-acetylamino)-propyl]-2-methanesulfonyloxy-6-methoxy-3,5-dimethyl-7-phenyl-hept-3-enyl ester

: 182222-83-9
N-[(2E,4E)-(1S,6S,7S)-1-((S)-1-[1,3]Dithian-2-yl-ethyl)-7-methoxy-4,6-dimethyl-8-phenyl-octa-2,4-dienyl]-2,2,2-trifluoro-acetamide

Guidance literature:: With anthracene radical anion sodium salt; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/0040-4039(96)01217-8

Reference yield:

: Trifluoro-acetic acid (2R,3S,4R,5S,6S)-4-azido-6-methoxy-2-((E)-(3S,4S)-4-methoxy-1,3-dimethyl-5-phenyl-pent-1-enyl)-5-methyl-tetrahydro-pyran-3-yl ester

: 182222-83-9
N-[(2E,4E)-(1S,6S,7S)-1-((S)-1-[1,3]Dithian-2-yl-ethyl)-7-methoxy-4,6-dimethyl-8-phenyl-octa-2,4-dienyl]-2,2,2-trifluoro-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / Pd/C / ethyl acetate

2: 98 percent / pyridine

3: BF₃*Et₂O / CH₂Cl₂

4: pyridine

5: 84 percent / Na-anthracene / tetrahydrofuran / 0 °C

With pyridine; boron trifluoride diethyl etherate; hydrogen; anthracene radical anion sodium salt; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1016/0040-4039(96)01217-8

Reference yield:

: 182369-24-0
(2R,3S,4R,5S,6S)-4-Azido-6-methoxy-2-((E)-(3S,4S)-4-methoxy-1,3-dimethyl-5-phenyl-pent-1-enyl)-5-methyl-tetrahydro-pyran-3-ol

: 182222-83-9
N-[(2E,4E)-(1S,6S,7S)-1-((S)-1-[1,3]Dithian-2-yl-ethyl)-7-methoxy-4,6-dimethyl-8-phenyl-octa-2,4-dienyl]-2,2,2-trifluoro-acetamide

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine

2: H₂ / Pd/C / ethyl acetate

3: 98 percent / pyridine

4: BF₃*Et₂O / CH₂Cl₂

5: pyridine

6: 84 percent / Na-anthracene / tetrahydrofuran / 0 °C

With pyridine; boron trifluoride diethyl etherate; hydrogen; anthracene radical anion sodium salt; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1016/0040-4039(96)01217-8