Technology Process of C32H48N2
There total 7 articles about C32H48N2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
ethanol; water; benzene;
at 90 ℃;
for 24h;
Inert atmosphere;
DOI:10.1021/ja200708b
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: palladium on carbon; hydrogen / acetic acid / 24 h
2.1: N-Bromosuccinimide; sodium sulfate; sodium hydrogencarbonate / chloroform / 3 h / -40 °C / Inert atmosphere
2.2: Inert atmosphere
3.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethanol; water; benzene / 24 h / 90 °C / Inert atmosphere
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); palladium on carbon; sodium sulfate; hydrogen; sodium hydrogencarbonate; sodium carbonate;
In
ethanol; chloroform; water; acetic acid; benzene;
3.1: Suzuki coupling;
DOI:10.1021/ja200708b
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N-Bromosuccinimide; sodium sulfate; sodium hydrogencarbonate / chloroform / 3 h / -40 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethanol; water; benzene / 24 h / 90 °C / Inert atmosphere
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); sodium sulfate; sodium hydrogencarbonate; sodium carbonate;
In
ethanol; chloroform; water; benzene;
2.1: Suzuki coupling;
DOI:10.1021/ja200708b
