Technology Process of C10H12O5S
There total 2 articles about C10H12O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C11H14O4S;
With
ozone;
In
dichloromethane;
at -78 ℃;
Inert atmosphere;
With
oxygen;
In
dichloromethane;
at -78 ℃;
for 2h;
Inert atmosphere;
With
dimethylsulfide;
In
dichloromethane;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1002/anie.201103950
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
2.1: ozone / dichloromethane / -78 °C / Inert atmosphere
2.2: 2 h / -78 °C / Inert atmosphere
2.3: 0 - 20 °C / Inert atmosphere
With
ozone; triethylamine;
In
dichloromethane;
DOI:10.1002/anie.201103950
- Guidance literature:
-
diethoxyphosphoryl-acetic acid ethyl ester;
With
sodium hydride;
In
tetrahydrofuran;
at 0 ℃;
for 0.833333h;
Inert atmosphere;
C10H12O5S;
In
tetrahydrofuran;
at 0 ℃;
for 0.75h;
optical yield given as %de;
Inert atmosphere;
DOI:10.1002/anie.201103950