C₂₀H₃₀INO₄S

Base Information

Chemical Name:C₂₀H₃₀INO₄S
CAS No.:1362120-13-5
Molecular Formula:C₂₀H₃₀INO₄S
Molecular Weight:507.433
Hs Code.:

C<sub>20</sub>H<sub>30</sub>INO<sub>4</sub>S

Synonyms:C₂₀H₃₀INO₄S

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Chemical Property of C₂₀H₃₀INO₄S

Chemical Property:

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Technology Process of C₂₀H₃₀INO₄S

There total 11 articles about C₂₀H₃₀INO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1362120-11-3
C₂₀H₃₁NO₅S

: 1362120-13-5
C₂₀H₃₀INO₄S

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 3.41667h;
DOI:10.1021/ol300342n

Reference yield:

: C₁₄H₂₅NO₃

: 1362120-13-5
C₂₀H₃₀INO₄S

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene-4-sulfonic acid / water; acetone / 0.33 h

2.1: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2.5 h

3.1: pivaloyl chloride; triethylamine / tetrahydrofuran / 3 h / -20 °C

3.2: 3.5 h / -20 - 20 °C

4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

4.2: 1 h / -78 °C

5.1: methanol; lithium borohydride / tetrahydrofuran / 2.67 h / 0 - 20 °C

6.1: ammonium molybdate; dihydrogen peroxide / ethanol; water / 12 h

7.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 3.42 h / 0 - 20 °C

With 1H-imidazole; methanol; sodium chlorite; lithium borohydride; ammonium molybdate; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; dihydrogen peroxide; iodine; sodium hexamethyldisilazane; pivaloyl chloride; toluene-4-sulfonic acid; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; water; acetone; tert-butyl alcohol; 2.1: Pinnick oxidation;
DOI:10.1021/ol300342n

Reference yield:

: C₁₃H₂₃NO₃

: 1362120-13-5
C₂₀H₃₀INO₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2.5 h

2.1: pivaloyl chloride; triethylamine / tetrahydrofuran / 3 h / -20 °C

2.2: 3.5 h / -20 - 20 °C

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

3.2: 1 h / -78 °C

4.1: methanol; lithium borohydride / tetrahydrofuran / 2.67 h / 0 - 20 °C

5.1: ammonium molybdate; dihydrogen peroxide / ethanol; water / 12 h

6.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 3.42 h / 0 - 20 °C

With 1H-imidazole; methanol; sodium chlorite; lithium borohydride; ammonium molybdate; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; dihydrogen peroxide; iodine; sodium hexamethyldisilazane; pivaloyl chloride; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; water; tert-butyl alcohol; 1.1: Pinnick oxidation;
DOI:10.1021/ol300342n