2,4-Dibromo-3,3-difluoro-8-(diphenylmethylene)tricyclo[3.2.1.0^2,4]oct-6-ene

Base Information

Chemical Name:2,4-Dibromo-3,3-difluoro-8-(diphenylmethylene)tricyclo[3.2.1.0^2,4]oct-6-ene
CAS No.:277755-64-3
Molecular Formula:C₂₁H₁₄Br₂F₂
Molecular Weight:464.147
Hs Code.:

2,4-Dibromo-3,3-difluoro-8-(diphenylmethylene)tricyclo[3.2.1.0<sup>2,4</sup>]oct-6-ene

Synonyms:2,4-Dibromo-3,3-difluoro-8-(diphenylmethylene)tricyclo[3.2.1.0^2,4]oct-6-ene

Suppliers and Price of 2,4-Dibromo-3,3-difluoro-8-(diphenylmethylene)tricyclo[3.2.1.0^2,4]oct-6-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,4-Dibromo-3,3-difluoro-8-(diphenylmethylene)tricyclo[3.2.1.0^2,4]oct-6-ene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,4-Dibromo-3,3-difluoro-8-(diphenylmethylene)tricyclo[3.2.1.0^2,4]oct-6-ene

There total 1 articles about 2,4-Dibromo-3,3-difluoro-8-(diphenylmethylene)tricyclo[3.2.1.0^2,4]oct-6-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 2175-90-8
6,6-Diphenylfulvene

: 6262-46-0
1,2-dibromo-3,3-difluorocyclopropene

: 277755-64-3
2,4-Dibromo-3,3-difluoro-8-(diphenylmethylene)tricyclo[3.2.1.0^2,4]oct-6-ene

Guidance literature:: In tetrachloromethane; at 120 ℃; for 15h;
DOI:10.1016/S0022-1139(99)00290-0

Reference yield: 58.8%

: 277755-64-3
2,4-Dibromo-3,3-difluoro-8-(diphenylmethylene)tricyclo[3.2.1.0^2,4]oct-6-ene

: 277755-65-4
2,4-Dibromo-3,3-difluoro-8-(diphenylmethylene)tricyclo[3.2.1.0^2,4]octane

Guidance literature:: With triethylamine; toluene-4-sulfonic acid hydrazide; In diethylene glycol dimethyl ether; at 80 ℃; for 24h;
DOI:10.1016/S0022-1139(99)00290-0

Reference yield:

: 277755-64-3
2,4-Dibromo-3,3-difluoro-8-(diphenylmethylene)tricyclo[3.2.1.0^2,4]oct-6-ene

: 3,3-Difluoro-8-(diphenylmethylene)tricyclo[3.2.1.0^2,4]octane

Guidance literature:: Multi-step reaction with 2 steps

1: 58.8 percent / p-toluenesulfonylhydrazine; Et₃N / bis-(2-methoxy-ethyl) ether / 24 h / 80 °C

2: 23 percent / tri-n-butyltin hydride; di-tert-butyl peroxide / 24 h / 90 °C

With di-tert-butyl peroxide; tri-n-butyl-tin hydride; triethylamine; toluene-4-sulfonic acid hydrazide; In diethylene glycol dimethyl ether; 1: Reduction / 2: Reduction;
DOI:10.1016/S0022-1139(99)00290-0