1,1,3,3-tetraphenylyloxy-5,5-bis(4-hydroxylmethylphenoxy)cyclotriphosphazene

Base Information

• Chemical Name: 1,1,3,3-tetraphenylyloxy-5,5-bis(4-hydroxylmethylphenoxy)cyclotriphosphazene
• CAS No.: 845540-58-1
• Molecular Formula: C₃₈H₃₀N₃O₈P₃
• Molecular Weight: 749.593
• Mol file: 845540-58-1.mol

Synonyms:1,1,3,3-tetraphenylyloxy-5,5-bis(4-hydroxylmethylphenoxy)cyclotriphosphazene

Chemical Property of 1,1,3,3-tetraphenylyloxy-5,5-bis(4-hydroxylmethylphenoxy)cyclotriphosphazene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 1,1,3,3-tetraphenylyloxy-5,5-bis(4-hydroxylmethylphenoxy)cyclotriphosphazene

There total 1 articles about 1,1,3,3-tetraphenylyloxy-5,5-bis(4-hydroxylmethylphenoxy)cyclotriphosphazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2,2-bis(4-formylphenoxy)-4,4,6,6-bis[spiro(2',2''-dioxy-1',1''-biphenylyl)]cyclotriphosphazene (916852-42-1) → 1,1,3,3-tetraphenylyloxy-5,5-bis(4-hydroxylmethylphenoxy)cyclotriphosphazene (845540-58-1)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 5h; Inert atmosphere;

DOI:10.1080/10426507.2011.583617

Reference yield: 80.0%

1,1,3,3-tetraphenylyloxy-5,5-bis(4-hydroxylmethylphenoxy)cyclotriphosphazene (845540-58-1) → bis(4-chloromethylphenoxy)-bis(2,2'-dihydroxybiphenyl)cyclotriphosphazene

Guidance literature:

With thionyl chloride; at 20 ℃; for 12h;

DOI:10.1002/chem.201400069

Reference yield: 72.4%

1,1,3,3-tetraphenylyloxy-5,5-bis(4-hydroxylmethylphenoxy)cyclotriphosphazene (845540-58-1) → 1,1,3,3-tetraphenylyloxy-5,5-bis(4-bromomethylphenoxy)cyclotriphosphazene (1349904-85-3)

Guidance literature:

With phosphorus tribromide; In tetrahydrofuran; at 0 ℃; for 5h; Inert atmosphere;

DOI:10.1080/10426507.2011.583617

upstream raw materials:

2,2-bis(4-formylphenoxy)-4,4,6,6-bis[spiro(2',2''-dioxy-1',1''-biphenylyl)]cyclotriphosphazene

Downstream raw materials:

1,1,3,3-tetraphenylyloxy-5,5-bis(4-bromomethylphenoxy)cyclotriphosphazene