methyl 3-hydroxy-2-[(4-{tert-butyldiphenylsilyloxy}butanoyl)amino]propanoate

Base Information Edit

Chemical Name:methyl 3-hydroxy-2-[(4-{tert-butyldiphenylsilyloxy}butanoyl)amino]propanoate
CAS No.:233750-49-7
Molecular Formula:C₂₄H₃₃NO₅Si
Molecular Weight:443.615
Hs Code.:
Mol file:233750-49-7.mol

Synonyms:methyl 3-hydroxy-2-[(4-{tert-butyldiphenylsilyloxy}butanoyl)amino]propanoate

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Chemical Property of methyl 3-hydroxy-2-[(4-{tert-butyldiphenylsilyloxy}butanoyl)amino]propanoate Edit

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Technology Process of methyl 3-hydroxy-2-[(4-{tert-butyldiphenylsilyloxy}butanoyl)amino]propanoate

There total 3 articles about methyl 3-hydroxy-2-[(4-{tert-butyldiphenylsilyloxy}butanoyl)amino]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₂₅O₃Si^(1-)*Na⁽¹⁺⁾

: 5619-04-5
methyl 2-amino-3-hydroxypropanoate hydrochloride

: 233750-49-7
methyl 3-hydroxy-2-[(4-{tert-butyldiphenylsilyloxy}butanoyl)amino]propanoate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In acetonitrile;
DOI:10.1016/j.bmcl.2011.10.109

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 233750-49-7
methyl 3-hydroxy-2-[(4-{tert-butyldiphenylsilyloxy}butanoyl)amino]propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / acetonitrile

With 1H-imidazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2011.10.109