N-benzyl-2-amino-6-O-benzyl-2,3-N,O-carbonyl-4-O-chloroacetyl-2-deoxy-α-D-glucopyranosyl bromide

Base Information

Chemical Name:N-benzyl-2-amino-6-O-benzyl-2,3-N,O-carbonyl-4-O-chloroacetyl-2-deoxy-α-D-glucopyranosyl bromide
CAS No.:910805-67-3
Molecular Formula:C₂₃H₂₃BrClNO₆
Molecular Weight:524.796
Hs Code.:

Synonyms:N-benzyl-2-amino-6-O-benzyl-2,3-N,O-carbonyl-4-O-chloroacetyl-2-deoxy-α-D-glucopyranosyl bromide

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Chemical Property of N-benzyl-2-amino-6-O-benzyl-2,3-N,O-carbonyl-4-O-chloroacetyl-2-deoxy-α-D-glucopyranosyl bromide

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Technology Process of N-benzyl-2-amino-6-O-benzyl-2,3-N,O-carbonyl-4-O-chloroacetyl-2-deoxy-α-D-glucopyranosyl bromide

There total 10 articles about N-benzyl-2-amino-6-O-benzyl-2,3-N,O-carbonyl-4-O-chloroacetyl-2-deoxy-α-D-glucopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 910805-52-6
phenyl N-benzyl-2-amino-6-O-benzyl-2,3-N,O-carbonyl-4-O-chloroacetyl-2-deoxy-1-thio-β-D-glucopyranoside

: 910805-67-3
N-benzyl-2-amino-6-O-benzyl-2,3-N,O-carbonyl-4-O-chloroacetyl-2-deoxy-α-D-glucopyranosyl bromide

Guidance literature:: With bromine; In dichloromethane; for 0.5h; cooling;
DOI:10.1021/ja062531e

Reference yield: 83.0%

: 910805-52-6
phenyl N-benzyl-2-amino-6-O-benzyl-2,3-N,O-carbonyl-4-O-chloroacetyl-2-deoxy-1-thio-β-D-glucopyranoside

: 910805-67-3
N-benzyl-2-amino-6-O-benzyl-2,3-N,O-carbonyl-4-O-chloroacetyl-2-deoxy-α-D-glucopyranosyl bromide

: 1268469-39-1
6-O-benzyl-2-benzylamino-2-N,3-O-carbonyl-4-O-chloroacetyl-2-deoxy-α-D-glucopyranosyl fluoride

Guidance literature:: With N-Bromosuccinimide; diethylamino-sulfur trifluoride; In dichloromethane; at -10 - 0 ℃;
DOI:10.1002/ejoc.201001278

Reference yield:

: 910805-50-4
phenyl N-benzyl-2-amino-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-β-D-glucopyranoside

: 910805-67-3
N-benzyl-2-amino-6-O-benzyl-2,3-N,O-carbonyl-4-O-chloroacetyl-2-deoxy-α-D-glucopyranosyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / pyridine / CH₂Cl₂ / 0.5 h / cooling

2: 91 percent / Br₂ / CH₂Cl₂ / 0.5 h / cooling

With pyridine; bromine; In dichloromethane;
DOI:10.1021/ja062531e