1,4-bis(5-(2'-butyl-1'-octyl)-2-thienyl)-2,5-bis(5-bromo-2-thienyl)benzene

Base Information

Chemical Name:1,4-bis(5-(2'-butyl-1'-octyl)-2-thienyl)-2,5-bis(5-bromo-2-thienyl)benzene
CAS No.:1271438-81-3
Molecular Formula:C₄₆H₆₀Br₂S₄
Molecular Weight:901.054
Hs Code.:

Synonyms:1,4-bis(5-(2'-butyl-1'-octyl)-2-thienyl)-2,5-bis(5-bromo-2-thienyl)benzene

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Chemical Property of 1,4-bis(5-(2'-butyl-1'-octyl)-2-thienyl)-2,5-bis(5-bromo-2-thienyl)benzene

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Technology Process of 1,4-bis(5-(2'-butyl-1'-octyl)-2-thienyl)-2,5-bis(5-bromo-2-thienyl)benzene

There total 4 articles about 1,4-bis(5-(2'-butyl-1'-octyl)-2-thienyl)-2,5-bis(5-bromo-2-thienyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.2%

: 1271438-77-7
1,4-bis(5-(2'-butyl-1'-octyl)-2-thienyl)-2,5-bis(2-thienyl)benzene

: 1271438-81-3
1,4-bis(5-(2'-butyl-1'-octyl)-2-thienyl)-2,5-bis(5-bromo-2-thienyl)benzene

Guidance literature:: With N-Bromosuccinimide; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere; Darkness;
DOI:10.1021/ja1110915

Reference yield:

: 1049822-69-6
1,4-bis(2-thienyl)-2,5-dibromobenzene

: 1271438-81-3
1,4-bis(5-(2'-butyl-1'-octyl)-2-thienyl)-2,5-bis(5-bromo-2-thienyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 48 h / 130 °C / Inert atmosphere

2: N-Bromosuccinimide / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere; Darkness

With bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ja1110915

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 1271438-81-3
1,4-bis(5-(2'-butyl-1'-octyl)-2-thienyl)-2,5-bis(5-bromo-2-thienyl)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid; iodine / 60 - 130 °C

2: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere

3: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 48 h / 130 °C / Inert atmosphere

4: N-Bromosuccinimide / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere; Darkness

With bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; sulfuric acid; iodine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ja1110915