(2R,4S,5S)-5-amino-N-bicyclo[2.2.1]hept-2-yl-4-hydroxy-2-methyl-6-phenylhexanamide

Base Information

Chemical Name:(2R,4S,5S)-5-amino-N-bicyclo[2.2.1]hept-2-yl-4-hydroxy-2-methyl-6-phenylhexanamide
CAS No.:537041-43-3
Molecular Formula:C₂₀H₃₀N₂O₂
Molecular Weight:330.47
Hs Code.:

Synonyms:(2R,4S,5S)-5-amino-N-bicyclo[2.2.1]hept-2-yl-4-hydroxy-2-methyl-6-phenylhexanamide

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Chemical Property of (2R,4S,5S)-5-amino-N-bicyclo[2.2.1]hept-2-yl-4-hydroxy-2-methyl-6-phenylhexanamide

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Technology Process of (2R,4S,5S)-5-amino-N-bicyclo[2.2.1]hept-2-yl-4-hydroxy-2-methyl-6-phenylhexanamide

There total 1 articles about (2R,4S,5S)-5-amino-N-bicyclo[2.2.1]hept-2-yl-4-hydroxy-2-methyl-6-phenylhexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 537041-41-1
1,1-dimethylethyl [(1S,2S,4R)-5-(bicyclo[2.2.1]hept-2-ylamino)-2-hydroxy-4-methyl-5-oxo-1-(phenylmethyl)pentyl]carbamate

: 537041-43-3
(2R,4S,5S)-5-amino-N-bicyclo[2.2.1]hept-2-yl-4-hydroxy-2-methyl-6-phenylhexanamide

Guidance literature:: 1,1-dimethylethyl [(1S,2S,4R)-5-(bicyclo[2.2.1]hept-2-ylamino)-2-hydroxy-4-methyl-5-oxo-1-(phenylmethyl)pentyl]carbamate; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2.5h;

With sodium hydrogencarbonate; In ethyl acetate;

Reference yield: 72.0%

: 138099-41-9
3-(1,1-dioxo-1,2-thiazolidin-2-yl)benzoic acid

: 537041-43-3
(2R,4S,5S)-5-amino-N-bicyclo[2.2.1]hept-2-yl-4-hydroxy-2-methyl-6-phenylhexanamide

: N-[(1S,2S,4R)-5-(bicyclo[2.2.1]hept-2-ylamino)-2-hydroxy-4-methyl-5-oxo-1-(phenylmethyl)pentyl]-3-(1,1-dioxido-2-isothiazolidinyl)benzamide

Guidance literature:: 3-(1,1-dioxo-1,2-thiazolidin-2-yl)benzoic acid; (2R,4S,5S)-5-amino-N-bicyclo[2.2.1]hept-2-yl-4-hydroxy-2-methyl-6-phenylhexanamide; With C₈H₁₃N₂Pol; benzotriazol-1-ol; In DMF (N,N-dimethyl-formamide); dichloromethane; at 20 ℃; Polystyrene

With tris(2-amimoethyl)amine polystyrene; polystyrene methyl isocyanate; In DMF (N,N-dimethyl-formamide); dichloromethane; for 1.5h;