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Technology Process of (C20H8N4Fe(OH))(F2(C6H3))3(C6H4)OCH2(C5H3N)CH2N(CH2(C5H4N))2

(C20H8N4Fe(OH))(F2(C6H3))3(C6H4)OCH2(C5H3N)CH2N(CH2(C5H4N))2

Base Information
  • Chemical Name:(C20H8N4Fe(OH))(F2(C6H3))3(C6H4)OCH2(C5H3N)CH2N(CH2(C5H4N))2
  • CAS No.:213403-81-7
  • Molecular Formula:C63H41F6FeN8O2
  • Molecular Weight:1111.91
  • Hs Code.:
(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>Fe(OH))(F<sub>2</sub>(C<sub>6</sub>H<sub>3</sub>))3(C<sub>6</sub>H<sub>4</sub>)OCH<sub>2</sub>(C<sub>5</sub>H<sub>3</sub>N)CH<sub>2</sub>N(CH<sub>2</sub>(C<sub>5</sub>H<sub>4</sub>N))2

Synonyms:(C20H8N4Fe(OH))(F2(C6H3))3(C6H4)OCH2(C5H3N)CH2N(CH2(C5H4N))2

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Chemical Property of (C20H8N4Fe(OH))(F2(C6H3))3(C6H4)OCH2(C5H3N)CH2N(CH2(C5H4N))2
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Technology Process of (C20H8N4Fe(OH))(F2(C6H3))3(C6H4)OCH2(C5H3N)CH2N(CH2(C5H4N))2

There total 4 articles about (C20H8N4Fe(OH))(F2(C6H3))3(C6H4)OCH2(C5H3N)CH2N(CH2(C5H4N))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(C<sub>20</sub>H<sub>10</sub>N<sub>4</sub>)(F<sub>2</sub>(C<sub>6</sub>H<sub>3</sub>))3(C<sub>6</sub>H<sub>4</sub>)OCH<sub>2</sub>(C<sub>5</sub>H<sub>3</sub>N)CH<sub>2</sub>N(CH<sub>2</sub>(C<sub>5</sub>H<sub>4</sub>N))2

(C20H10N4)(F2(C6H3))3(C6H4)OCH2(C5H3N)CH2N(CH2(C5H4N))2

iron(II) chloride

iron(II) chloride

(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>Fe(OH))(F<sub>2</sub>(C<sub>6</sub>H<sub>3</sub>))3(C<sub>6</sub>H<sub>4</sub>)OCH<sub>2</sub>(C<sub>5</sub>H<sub>3</sub>N)CH<sub>2</sub>N(CH<sub>2</sub>(C<sub>5</sub>H<sub>4</sub>N))2
213403-81-7

(C20H8N4Fe(OH))(F2(C6H3))3(C6H4)OCH2(C5H3N)CH2N(CH2(C5H4N))2

Guidance literature:
With air; In not given; treatment of ligand with excess FeCl2, then with air, then with base or Me3SiCl; chromy.;
DOI:10.1021/ic9900511

Reference yield:

iron(II) chloride tetrahydrate

iron(II) chloride tetrahydrate

(C<sub>20</sub>H<sub>10</sub>N<sub>4</sub>)(F<sub>2</sub>(C<sub>6</sub>H<sub>3</sub>))3(C<sub>6</sub>H<sub>4</sub>)OCH<sub>2</sub>(C<sub>5</sub>H<sub>3</sub>N)CH<sub>2</sub>N(CH<sub>2</sub>(C<sub>5</sub>H<sub>4</sub>N))2

(C20H10N4)(F2(C6H3))3(C6H4)OCH2(C5H3N)CH2N(CH2(C5H4N))2

sodium hydroxide
1310-73-2

sodium hydroxide

(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>Fe(OH))(F<sub>2</sub>(C<sub>6</sub>H<sub>3</sub>))3(C<sub>6</sub>H<sub>4</sub>)OCH<sub>2</sub>(C<sub>5</sub>H<sub>3</sub>N)CH<sub>2</sub>N(CH<sub>2</sub>(C<sub>5</sub>H<sub>4</sub>N))2
213403-81-7

(C20H8N4Fe(OH))(F2(C6H3))3(C6H4)OCH2(C5H3N)CH2N(CH2(C5H4N))2

Guidance literature:
With air; In N,N-dimethyl-formamide; org. ligand dissolved under Ar; purged with Ar (30 min); warmed; FeCl2*4H2O added under Ar; kept (2.5 h); exposed to air; cooled to room temp.; DMF removed; dissolved in CH2Cl2; added to satd. NaOH (stirring); stirred overnight; org. layer dried over Na2SO4; adsorbed onto Al2O3; column chromy. (1:1 hexane/ethyl acetate);
DOI:10.1016/j.ica.2007.08.016

Reference yield:

Fe(C<sub>5</sub>H<sub>2</sub>NC<sub>6</sub>H<sub>3</sub>F<sub>2</sub>)3C<sub>5</sub>H<sub>2</sub>NC<sub>6</sub>H<sub>4</sub>OCH<sub>2</sub>C<sub>5</sub>H<sub>3</sub>NCH<sub>2</sub>N(CH<sub>2</sub>C<sub>5</sub>H<sub>4</sub>N)2O<sub>2</sub>

Fe(C5H2NC6H3F2)3C5H2NC6H4OCH2C5H3NCH2N(CH2C5H4N)2O2

(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>Fe(OH))(F<sub>2</sub>(C<sub>6</sub>H<sub>3</sub>))3(C<sub>6</sub>H<sub>4</sub>)OCH<sub>2</sub>(C<sub>5</sub>H<sub>3</sub>N)CH<sub>2</sub>N(CH<sub>2</sub>(C<sub>5</sub>H<sub>4</sub>N))2
213403-81-7

(C20H8N4Fe(OH))(F2(C6H3))3(C6H4)OCH2(C5H3N)CH2N(CH2(C5H4N))2

Guidance literature:
In dichloromethane; (Ar); warming a soln. of iron complex in CH2Cl2 above 193 K; not isolated, detected by UV;
DOI:10.1021/ic0103547
upstream raw materials:

sodium hydroxide

Downstream raw materials:

Fe(C20H8N4(C6H3F2)3(C6H4OCH2C5H3NCH2N(CH2C5H4N)2))

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