2(S)-(ethoxycarbonylamino)-3,3-bis(1'H,1'H,2'H,2'H-perfluorooctyl)-1-phenyl-propan-3-ol

Base Information

Chemical Name:2(S)-(ethoxycarbonylamino)-3,3-bis(1'H,1'H,2'H,2'H-perfluorooctyl)-1-phenyl-propan-3-ol
CAS No.:871210-08-1
Molecular Formula:C₂₈H₂₃F₂₆NO₃
Molecular Weight:915.454
Hs Code.:

Synonyms:2(S)-(ethoxycarbonylamino)-3,3-bis(1'H,1'H,2'H,2'H-perfluorooctyl)-1-phenyl-propan-3-ol

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Chemical Property of 2(S)-(ethoxycarbonylamino)-3,3-bis(1'H,1'H,2'H,2'H-perfluorooctyl)-1-phenyl-propan-3-ol

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Technology Process of 2(S)-(ethoxycarbonylamino)-3,3-bis(1'H,1'H,2'H,2'H-perfluorooctyl)-1-phenyl-propan-3-ol

There total 4 articles about 2(S)-(ethoxycarbonylamino)-3,3-bis(1'H,1'H,2'H,2'H-perfluorooctyl)-1-phenyl-propan-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 91084-05-8
methyl (S)-2-ethyloxycarbonylamino-3-phenylpropanoate

: 871210-02-5
2(S)-(ethoxycarbonylamino)-6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-1-phenyl-undecan-3-one

: 871210-08-1
2(S)-(ethoxycarbonylamino)-3,3-bis(1'H,1'H,2'H,2'H-perfluorooctyl)-1-phenyl-propan-3-ol

Guidance literature:: 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane; With magnesium; In diethyl ether; for 90h;

methyl (S)-2-ethyloxycarbonylamino-3-phenylpropanoate; In diethyl ether; for 4h; Product distribution / selectivity;

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 871210-08-1
2(S)-(ethoxycarbonylamino)-3,3-bis(1'H,1'H,2'H,2'H-perfluorooctyl)-1-phenyl-propan-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 99 percent / SOCl₂ / 4 h / Heating

2.1: 87 percent / triethylamine / tetrahydrofuran / 0 - 20 °C

3.1: Mg / diethyl ether

3.2: diethyl ether / 4 h

With thionyl chloride; magnesium; triethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo051696n

Reference yield:

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 871210-08-1
2(S)-(ethoxycarbonylamino)-3,3-bis(1'H,1'H,2'H,2'H-perfluorooctyl)-1-phenyl-propan-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 87 percent / triethylamine / tetrahydrofuran / 0 - 20 °C

2.1: Mg / diethyl ether

2.2: diethyl ether / 4 h

With magnesium; triethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo051696n