6-endo-Methyl-8-exo-<3-(phenylsulfonyl)propyl>-2-endo-propyl-7-oxa-1-azabicyclo<3.2.1>octane

Base Information

Chemical Name:6-endo-Methyl-8-exo-<3-(phenylsulfonyl)propyl>-2-endo-propyl-7-oxa-1-azabicyclo<3.2.1>octane
CAS No.:120447-72-5
Molecular Formula:C₁₉H₂₉NO₃S
Molecular Weight:351.51
Hs Code.:

Synonyms:6-endo-Methyl-8-exo-<3-(phenylsulfonyl)propyl>-2-endo-propyl-7-oxa-1-azabicyclo<3.2.1>octane

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Chemical Property of 6-endo-Methyl-8-exo-<3-(phenylsulfonyl)propyl>-2-endo-propyl-7-oxa-1-azabicyclo<3.2.1>octane

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Technology Process of 6-endo-Methyl-8-exo-<3-(phenylsulfonyl)propyl>-2-endo-propyl-7-oxa-1-azabicyclo<3.2.1>octane

There total 8 articles about 6-endo-Methyl-8-exo-<3-(phenylsulfonyl)propyl>-2-endo-propyl-7-oxa-1-azabicyclo<3.2.1>octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3112-85-4
methylphenylsulfonate

: 120447-72-5
6-endo-Methyl-8-exo-<3-(phenylsulfonyl)propyl>-2-endo-propyl-7-oxa-1-azabicyclo<3.2.1>octane

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) n-butyllithium / 1.) THF, hexane, 0 deg C, 20 min; 2.) -78 deg C -> room temp., 3 h

2: 80 percent / HCl / acetone; H₂O / 3 h / Ambient temperature

3: Na₂SO₄ / benzene / 0 - 10 °C

4: benzene / 10 h / Heating

With hydrogenchloride; n-butyllithium; sodium sulfate; In water; acetone; benzene;
DOI:10.1021/ja00191a038

Reference yield:

: 120447-74-7
(Z)-7-Nonen-4-one

: 120447-72-5
6-endo-Methyl-8-exo-<3-(phenylsulfonyl)propyl>-2-endo-propyl-7-oxa-1-azabicyclo<3.2.1>octane

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / hydroxylamine hydrochloride, sodium acetate / aq. ethanol

2: 92 percent / sodium cyanoborohydride, 50percent methanolic HCl / methanol

3: Na₂SO₄ / benzene / 0 - 10 °C

4: benzene / 10 h / Heating

With hydrogenchloride; hydroxylamine hydrochloride; sodium acetate; sodium cyanoborohydride; sodium sulfate; In methanol; ethanol; benzene;
DOI:10.1021/ja00191a038

Reference yield:

: 120447-86-1
(Z)-7-Nonen-4-one oxime

: 120447-72-5
6-endo-Methyl-8-exo-<3-(phenylsulfonyl)propyl>-2-endo-propyl-7-oxa-1-azabicyclo<3.2.1>octane

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / sodium cyanoborohydride, 50percent methanolic HCl / methanol

2: Na₂SO₄ / benzene / 0 - 10 °C

3: benzene / 10 h / Heating

With hydrogenchloride; sodium cyanoborohydride; sodium sulfate; In methanol; benzene;
DOI:10.1021/ja00191a038