tert-butylmethyl ((S)-1-oxo-1-((3S,6S,10aS)-5-oxo-3-((R)-1-phenylprop-2-ynylcarbamoyl)decahydropyrrolo[1,2-a]azocin-6-ylamino)propan-2-yl)carbamate

Base Information

• Chemical Name: tert-butylmethyl ((S)-1-oxo-1-((3S,6S,10aS)-5-oxo-3-((R)-1-phenylprop-2-ynylcarbamoyl)decahydropyrrolo[1,2-a]azocin-6-ylamino)propan-2-yl)carbamate
• CAS No.: 957134-91-7
• Molecular Formula: C₂₉H₄₀N₄O₅
• Molecular Weight: 524.66

Synonyms:tert-butylmethyl ((S)-1-oxo-1-((3S,6S,10aS)-5-oxo-3-((R)-1-phenylprop-2-ynylcarbamoyl)decahydropyrrolo[1,2-a]azocin-6-ylamino)propan-2-yl)carbamate

Chemical Property of tert-butylmethyl ((S)-1-oxo-1-((3S,6S,10aS)-5-oxo-3-((R)-1-phenylprop-2-ynylcarbamoyl)decahydropyrrolo[1,2-a]azocin-6-ylamino)propan-2-yl)carbamate

Chemical Property:

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Technology Process of tert-butylmethyl ((S)-1-oxo-1-((3S,6S,10aS)-5-oxo-3-((R)-1-phenylprop-2-ynylcarbamoyl)decahydropyrrolo[1,2-a]azocin-6-ylamino)propan-2-yl)carbamate

There total 1 articles about tert-butylmethyl ((S)-1-oxo-1-((3S,6S,10aS)-5-oxo-3-((R)-1-phenylprop-2-ynylcarbamoyl)decahydropyrrolo[1,2-a]azocin-6-ylamino)propan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C20H25N3O2 + N-(tert-butoxycarbonyl)-N-methyl-L-alanine (16948-16-6) → tert-butylmethyl ((S)-1-oxo-1-((3S,6S,10aS)-5-oxo-3-((R)-1-phenylprop-2-ynylcarbamoyl)decahydropyrrolo[1,2-a]azocin-6-ylamino)propan-2-yl)carbamate (957134-91-7)

Guidance literature:

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In dichloromethane;

DOI:10.1021/ja074725f

Reference yield: 62.0%

1,4-bis-(4-azidobutyl)benzene (957136-19-5) + tert-butylmethyl ((S)-1-oxo-1-((3S,6S,10aS)-5-oxo-3-((R)-1-phenylprop-2-ynylcarbamoyl)decahydropyrrolo[1,2-a]azocin-6-ylamino)propan-2-yl)carbamate (957134-91-7) → tert-butyl ((S)-1-(((3S,6S,10aS)-3-(((1-(4-(4-(4-azidobutyl)phenyl)butyl)-1H-1,2,3-triazol-4-yl)(phenyl)methyl)carbamoyl)-5-oxodecahydropyrrolo[1,2-a]azocin-6-yl)amino)-1-oxopropan-2-yl)(methyl)carbamate (1298048-85-7)

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃;

DOI:10.1021/jm101651b

Reference yield:

1,4-bis-(4-azidobutyl)benzene (957136-19-5) + tert-butylmethyl ((S)-1-oxo-1-((3S,6S,10aS)-5-oxo-3-((R)-1-phenylprop-2-ynylcarbamoyl)decahydropyrrolo[1,2-a]azocin-6-ylamino)propan-2-yl)carbamate (957134-91-7) → C72H100N14O10

Guidance literature:

With copper(II) sulfate; In water; tert-butyl alcohol; at 20 ℃;

DOI:10.1021/ja074725f

upstream raw materials:

N-(tert-butoxycarbonyl)-N-methyl-L-alanine

Downstream raw materials:

tert-butyl ((S)-1-(((3S,6S,10aS)-3-(((1-(4-(4-(4-azidobutyl)phenyl)butyl)-1H-1,2,3-triazol-4-yl)(phenyl)methyl)carbamoyl)-5-oxodecahydropyrrolo[1,2-a]azocin-6-yl)amino)-1-oxopropan-2-yl)(methyl)carbamate

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