sodium 3-[4-(((α-D-mannopyranosyl)oxy)methyl)-1H-1,2,3-triazol-1-yl]benzoate

Base Information

Chemical Name:sodium 3-[4-(((α-D-mannopyranosyl)oxy)methyl)-1H-1,2,3-triazol-1-yl]benzoate
CAS No.:1345019-10-4
Molecular Formula:C₁₆H₁₈N₃O₈*Na
Molecular Weight:403.324
Hs Code.:

Synonyms:sodium 3-[4-(((α-D-mannopyranosyl)oxy)methyl)-1H-1,2,3-triazol-1-yl]benzoate

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Chemical Property of sodium 3-[4-(((α-D-mannopyranosyl)oxy)methyl)-1H-1,2,3-triazol-1-yl]benzoate

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Technology Process of sodium 3-[4-(((α-D-mannopyranosyl)oxy)methyl)-1H-1,2,3-triazol-1-yl]benzoate

There total 2 articles about sodium 3-[4-(((α-D-mannopyranosyl)oxy)methyl)-1H-1,2,3-triazol-1-yl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1345018-87-2
ethyl 3-[4-(((2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)oxy)methyl)-1H-1,2,3-triazol-1-yl]benzoate

: 1345019-10-4
sodium 3-[4-(((α-D-mannopyranosyl)oxy)methyl)-1H-1,2,3-triazol-1-yl]benzoate

Guidance literature:: ethyl 3-[4-(((2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)oxy)methyl)-1H-1,2,3-triazol-1-yl]benzoate; With methanol; sodium methylate; at 20 ℃; for 3h; Inert atmosphere;

With sodium hydroxide; In 1,4-dioxane; water; for 16h;
DOI:10.1016/j.bmc.2011.08.057

Reference yield:

: 83476-52-2
propargyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

: 56423-50-8
3-azido benzoic acid ethyl ester

: 1345019-10-4
sodium 3-[4-(((α-D-mannopyranosyl)oxy)methyl)-1H-1,2,3-triazol-1-yl]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water; tert-butyl alcohol / 24 h / 20 °C / Inert atmosphere

2.1: methanol; sodium methylate / 3 h / 20 °C / Inert atmosphere

2.2: 16 h

With methanol; copper(ll) sulfate pentahydrate; sodium methylate; sodium L-ascorbate; In tetrahydrofuran; water; tert-butyl alcohol; 1.1: Huisgen 1,3-dipolar cycloaddition / 2.1: Zemplen deacetylation;
DOI:10.1016/j.bmc.2011.08.057