N-benzyl-N-{2-[(tert-butyl)amino]-1-(2-chlorophenyl)-2-oxoethyl}-2-chloroacetamide

Base Information

Chemical Name:N-benzyl-N-{2-[(tert-butyl)amino]-1-(2-chlorophenyl)-2-oxoethyl}-2-chloroacetamide
CAS No.:1370472-07-3
Molecular Formula:C₂₁H₂₄Cl₂N₂O₂
Molecular Weight:407.34
Hs Code.:

Synonyms:N-benzyl-N-{2-[(tert-butyl)amino]-1-(2-chlorophenyl)-2-oxoethyl}-2-chloroacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-N-{2-[(tert-butyl)amino]-1-(2-chlorophenyl)-2-oxoethyl}-2-chloroacetamide

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Technology Process of N-benzyl-N-{2-[(tert-butyl)amino]-1-(2-chlorophenyl)-2-oxoethyl}-2-chloroacetamide

There total 1 articles about N-benzyl-N-{2-[(tert-butyl)amino]-1-(2-chlorophenyl)-2-oxoethyl}-2-chloroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 89-98-5
2-chloro-benzaldehyde

: 79-11-8
chloroacetic acid

: 100-46-9
benzylamine

: 1370472-07-3
N-benzyl-N-{2-[(tert-butyl)amino]-1-(2-chlorophenyl)-2-oxoethyl}-2-chloroacetamide

Guidance literature:: 2-chloro-benzaldehyde; benzylamine; In dichloromethane; at 20 ℃; for 0.333333h;

tert-butylisonitrile; chloroacetic acid; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1016/j.bmcl.2012.01.111

Reference yield: 81.0%

: 1370472-07-3
N-benzyl-N-{2-[(tert-butyl)amino]-1-(2-chlorophenyl)-2-oxoethyl}-2-chloroacetamide

: 1370471-18-3
2-azido-N-benzyl-N-{2-[(tert-butyl)amino]-1-(2-chlorophenyl)-2-oxoethyl}-2-acetamide

Guidance literature:: With sodium azide; potassium carbonate; In N,N-dimethyl acetamide; at 20 ℃; for 4h;
DOI:10.1002/hlca.201300057

Reference yield:

: 1370472-07-3
N-benzyl-N-{2-[(tert-butyl)amino]-1-(2-chlorophenyl)-2-oxoethyl}-2-chloroacetamide

: N-benzyl-N-{2-[(tert-butyl)amino]-1-(2-chlorophenyl)-2-oxoethyl}-2-[4-({2-methoxy-4-[(Z)-(5-oxo-2-phenyl-1,3-oxazol-4(5H)-ylidene)methyl]phenoxy}methyl)-1H-1,2,3-triazol-1-yl]acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide; potassium carbonate / N,N-dimethyl acetamide / 4 h / 20 °C

2: sodium L-ascorbate; copper(ll) sulfate pentahydrate / dimethyl sulfoxide; tert-butyl alcohol; water / 24 h / 20 °C

With sodium azide; copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate; In N,N-dimethyl acetamide; water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1002/hlca.201300057