Technology Process of C25H21NO
There total 3 articles about C25H21NO which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ethanol; hydroxylamine hydrochloride; water;
for 19h;
Reflux;
DOI:10.1246/cl.2012.625
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 19 h / 60 °C
2: ethanol; hydroxylamine hydrochloride; water / 19 h / Reflux
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; ethanol; hydroxylamine hydrochloride; water; triethylamine; triphenylphosphine;
In
tetrahydrofuran;
DOI:10.1246/cl.2012.625
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 19 h / 60 °C
2: ethanol; hydroxylamine hydrochloride; water / 19 h / Reflux
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; ethanol; hydroxylamine hydrochloride; water; triethylamine; triphenylphosphine;
In
tetrahydrofuran;
DOI:10.1246/cl.2012.625