dihydrido(η-cyclopentadienyl)bis(triphenylphosphine)osmium(IV)triiodide

Base Information

Chemical Name:dihydrido(η-cyclopentadienyl)bis(triphenylphosphine)osmium(IV)triiodide
CAS No.:112142-94-6
Molecular Formula:C₄₁H₃₇OsP₂*I₃
Molecular Weight:1162.61
Hs Code.:

Synonyms:dihydrido(η-cyclopentadienyl)bis(triphenylphosphine)osmium(IV)triiodide

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Chemical Property of dihydrido(η-cyclopentadienyl)bis(triphenylphosphine)osmium(IV)triiodide

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Technology Process of dihydrido(η-cyclopentadienyl)bis(triphenylphosphine)osmium(IV)triiodide

There total 2 articles about dihydrido(η-cyclopentadienyl)bis(triphenylphosphine)osmium(IV)triiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 34742-23-9
(η5-cyclopentadienyl)bis(triphenylphosphine)osmium(II)(Br)

: 112142-94-6
dihydrido(η-cyclopentadienyl)bis(triphenylphosphine)osmium(IV)triiodide

Guidance literature:: With iodine; potassium iodide; In methanol; ethylene glycol; CpOsBr(PPh3)2 refluxed in ethylene glycol, after cooling added MeOH, mixture (I2, KI, H2O, MeOH) added to soln.; after 20 min filtered, washed with MeOH, n-hexane, dried;
DOI:10.1016/0022-328X(86)80542-3

Reference yield: 74.0%

: (η5-C5H5)OsH(PPh3)2

: 112142-94-6
dihydrido(η-cyclopentadienyl)bis(triphenylphosphine)osmium(IV)triiodide

Guidance literature:: With hydrogen iodide; iodine; In methanol; CpOsH(PPh3)2 added to a soln. of I2, HI in MeOH, heated at 40°C with stirring for 15 min; filtered, washed, dried;
DOI:10.1016/0022-328X(86)80542-3