2,4,4-trimethyl-3,5-di-t-butyl-7-phenyl-2-alumina-3,5-diaza-4-sila-6-magnesiaheptane

Base Information

Chemical Name:2,4,4-trimethyl-3,5-di-t-butyl-7-phenyl-2-alumina-3,5-diaza-4-sila-6-magnesiaheptane
CAS No.:114008-91-2
Molecular Formula:C₁₉H₃₇AlMgN₂Si
Molecular Weight:372.888
Hs Code.:

Synonyms:2,4,4-trimethyl-3,5-di-t-butyl-7-phenyl-2-alumina-3,5-diaza-4-sila-6-magnesiaheptane

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Chemical Property of 2,4,4-trimethyl-3,5-di-t-butyl-7-phenyl-2-alumina-3,5-diaza-4-sila-6-magnesiaheptane

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Technology Process of 2,4,4-trimethyl-3,5-di-t-butyl-7-phenyl-2-alumina-3,5-diaza-4-sila-6-magnesiaheptane

There total 2 articles about 2,4,4-trimethyl-3,5-di-t-butyl-7-phenyl-2-alumina-3,5-diaza-4-sila-6-magnesiaheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.2%

: 2,4,4-trimethyl-3,5-di-t-butyl-2-alumina-3,5-diaza-4-sila-6-sodiahexane

: 114008-91-2
2,4,4-trimethyl-3,5-di-t-butyl-7-phenyl-2-alumina-3,5-diaza-4-sila-6-magnesiaheptane

Guidance literature:: With PhCH₂MgX; In diethyl ether; toluene; a soln. of PhCH2MgX was added to a soln. of Na-compound in toluene-Et2Ounder N2, mixt. was stirred for 24 h; evapd., residue was treated with toluene, filtered, volatiles removed; elem. anal.;
DOI:10.1016/0022-328X(87)87003-1

Reference yield:

: 97683-82-4
(CH₃)3CNHSi(CH₃)2N(Al(CH₃)2)C(CH₃)3

: 114008-91-2
2,4,4-trimethyl-3,5-di-t-butyl-7-phenyl-2-alumina-3,5-diaza-4-sila-6-magnesiaheptane

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether; hexane

2: PhCH₂MgX / toluene; diethyl ether

With PhCH₂MgX; In diethyl ether; hexane; toluene;
DOI:10.1016/0022-328X(87)87003-1