di-tert-butyl 5-cyclohexyl-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate

Base Information

Chemical Name:di-tert-butyl 5-cyclohexyl-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate
CAS No.:1319727-26-8
Molecular Formula:C₂₆H₃₄N₂O₆
Molecular Weight:470.566
Hs Code.:

Synonyms:di-tert-butyl 5-cyclohexyl-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate

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Chemical Property of di-tert-butyl 5-cyclohexyl-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate

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Technology Process of di-tert-butyl 5-cyclohexyl-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate

There total 3 articles about di-tert-butyl 5-cyclohexyl-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 66086-33-7
Di-tert-butyl acetylenedicarboxylate

: 1319727-20-2
2-cyclohexyl-2-(4-nitrobenzylideneamino)acetonitrile

: 1319727-26-8
di-tert-butyl 5-cyclohexyl-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 0.0166667h; Microwave irradiation;
DOI:10.1055/s-0030-1260415

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 1319727-26-8
di-tert-butyl 5-cyclohexyl-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: ammonia; ammonium chloride / ethanol / 1.5 h / 20 °C

2: magnesium sulfate; acetic acid / dichloromethane / 20 °C / Inert atmosphere

3: caesium carbonate / N,N-dimethyl-formamide / 0.02 h / 100 °C / Microwave irradiation

With ammonia; magnesium sulfate; ammonium chloride; caesium carbonate; acetic acid; In ethanol; dichloromethane; N,N-dimethyl-formamide; 1: Strecker reaction;
DOI:10.1055/s-0030-1260415

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 40651-95-4
2-amino-2-cyclohexylacetonitrile

: 1319727-26-8
di-tert-butyl 5-cyclohexyl-2-(4-nitrophenyl)-1H-pyrrole-3,4-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium sulfate; acetic acid / dichloromethane / 20 °C / Inert atmosphere

2: caesium carbonate / N,N-dimethyl-formamide / 0.02 h / 100 °C / Microwave irradiation

With magnesium sulfate; caesium carbonate; acetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-0030-1260415