3,5-bis(4-diphenylaminophenylethynyl)phenylethynyldiphenylphosphine oxide

Base Information

Chemical Name:3,5-bis(4-diphenylaminophenylethynyl)phenylethynyldiphenylphosphine oxide
CAS No.:1351165-80-4
Molecular Formula:C₆₀H₄₁N₂OP
Molecular Weight:836.972
Hs Code.:

Synonyms:3,5-bis(4-diphenylaminophenylethynyl)phenylethynyldiphenylphosphine oxide

Suppliers and Price of 3,5-bis(4-diphenylaminophenylethynyl)phenylethynyldiphenylphosphine oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3,5-bis(4-diphenylaminophenylethynyl)phenylethynyldiphenylphosphine oxide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of 3,5-bis(4-diphenylaminophenylethynyl)phenylethynyldiphenylphosphine oxide

There total 5 articles about 3,5-bis(4-diphenylaminophenylethynyl)phenylethynyldiphenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 38257-52-2
4-(N,N-diphenylamino)iodobenzene

: 1351165-70-2
C₂₄H₁₅OP

: 1351165-80-4
3,5-bis(4-diphenylaminophenylethynyl)phenylethynyldiphenylphosphine oxide

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine; In toluene; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1055/s-0030-1261223

Reference yield: 77.0%

: 1351165-70-2
C₂₄H₁₅OP

: 205877-26-5
4-diphenylaminophenylacetylene

: 1351165-80-4
3,5-bis(4-diphenylaminophenylethynyl)phenylethynyldiphenylphosphine oxide

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine; In toluene; at 20 ℃; for 12h;
DOI:10.1246/bcsj.20110390

Reference yield:

: C₂₄H₁₅P

: 1351165-80-4
3,5-bis(4-diphenylaminophenylethynyl)phenylethynyldiphenylphosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide / tetrahydrofuran; water / 20 °C / Inert atmosphere

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine / toluene / 12 h / 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dihydrogen peroxide; diisopropylamine; In tetrahydrofuran; water; toluene; 2: Sonogashira coupling;
DOI:10.1055/s-0030-1261223