tert-butyl 3-(hydroxy(2-(pyrrolidin-1-ylsulfonyl)phenyl)methyl)-2-methyl-4-oxo-6,7-dihydro-1H-pyrrolo[3,2-c]pyridine-5(4H)-carboxylate

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Chemical Name:tert-butyl 3-(hydroxy(2-(pyrrolidin-1-ylsulfonyl)phenyl)methyl)-2-methyl-4-oxo-6,7-dihydro-1H-pyrrolo[3,2-c]pyridine-5(4H)-carboxylate
CAS No.:1355961-46-4
Molecular Formula:C₂₄H₃₁N₃O₆S
Molecular Weight:489.593
Hs Code.:

Synonyms:tert-butyl 3-(hydroxy(2-(pyrrolidin-1-ylsulfonyl)phenyl)methyl)-2-methyl-4-oxo-6,7-dihydro-1H-pyrrolo[3,2-c]pyridine-5(4H)-carboxylate

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Chemical Property of tert-butyl 3-(hydroxy(2-(pyrrolidin-1-ylsulfonyl)phenyl)methyl)-2-methyl-4-oxo-6,7-dihydro-1H-pyrrolo[3,2-c]pyridine-5(4H)-carboxylate

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Technology Process of tert-butyl 3-(hydroxy(2-(pyrrolidin-1-ylsulfonyl)phenyl)methyl)-2-methyl-4-oxo-6,7-dihydro-1H-pyrrolo[3,2-c]pyridine-5(4H)-carboxylate

There total 1 articles about tert-butyl 3-(hydroxy(2-(pyrrolidin-1-ylsulfonyl)phenyl)methyl)-2-methyl-4-oxo-6,7-dihydro-1H-pyrrolo[3,2-c]pyridine-5(4H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 845267-78-9
tert-butyl 2,4-dioxopiperidine-1-carboxylate

: 1355961-46-4
tert-butyl 3-(hydroxy(2-(pyrrolidin-1-ylsulfonyl)phenyl)methyl)-2-methyl-4-oxo-6,7-dihydro-1H-pyrrolo[3,2-c]pyridine-5(4H)-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonium acetate / ethanol / 0.08 h / 20 °C

1.2: 14 h / 20 °C

2.1: sodium hydroxide / 2,2,2-trifluoroethanol / 14 h / 90 °C

With ammonium acetate; sodium hydroxide; In ethanol; 2,2,2-trifluoroethanol;

Reference yield:

: 1355961-46-4
tert-butyl 3-(hydroxy(2-(pyrrolidin-1-ylsulfonyl)phenyl)methyl)-2-methyl-4-oxo-6,7-dihydro-1H-pyrrolo[3,2-c]pyridine-5(4H)-carboxylate

: 1355961-41-9
2-methyl-3-(2-(pyrrolidin-1-ylsulfonyl)benzyl)-6,7-dihydro-1H-pyrrolo[3,2-c]pyridin-4(5H)-one

Guidance literature:: tert-butyl 3-(hydroxy(2-(pyrrolidin-1-ylsulfonyl)phenyl)methyl)-2-methyl-4-oxo-6,7-dihydro-1H-pyrrolo[3,2-c]pyridine-5(4H)-carboxylate; With triethylsilane; trifluoroacetic acid; In dichloromethane; at -78 - 20 ℃;

With sodium hydrogencarbonate; In dichloromethane;

Reference yield:

: 1355961-46-4
tert-butyl 3-(hydroxy(2-(pyrrolidin-1-ylsulfonyl)phenyl)methyl)-2-methyl-4-oxo-6,7-dihydro-1H-pyrrolo[3,2-c]pyridine-5(4H)-carboxylate

: 1355959-76-0
2-(2-methyl-4-oxo-3-(2-(pyrrolidin-1-ylsulfonyl)benzyl)-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid; triethylsilane / dichloromethane / -78 - 20 °C

2: potassium carbonate / acetonitrile / 50 °C

3: water; lithium hydroxide / tetrahydrofuran; methanol / 1 h / 20 °C

With triethylsilane; water; potassium carbonate; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;