3-(2-bromoacetamido)propyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

Base Information

Chemical Name:3-(2-bromoacetamido)propyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside
CAS No.:866028-76-4
Molecular Formula:C₃₉H₃₆BrNO₁₁
Molecular Weight:774.619
Hs Code.:

Synonyms:3-(2-bromoacetamido)propyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

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Chemical Property of 3-(2-bromoacetamido)propyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

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Technology Process of 3-(2-bromoacetamido)propyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

There total 3 articles about 3-(2-bromoacetamido)propyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 866028-71-9
2-bromo-N-(3-hydroxypropyl)acetamide

: 14218-11-2,14218-30-5,61198-88-7,108438-33-1,108836-02-8,114682-36-9,127305-34-4,151377-77-4
2,3,4,6-Tetra-O-benzoyl-α-D-mannopyranosyl bromide

: 866028-76-4
3-(2-bromoacetamido)propyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

Guidance literature:: With iodine; In acetonitrile; at 20 ℃; for 3h;
DOI:10.1002/ejoc.200500146

Reference yield:

: 866028-74-2
3-[(benzyloxycarbonyl)amino]propyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

: 866028-76-4
3-(2-bromoacetamido)propyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / acetic acid; ethyl acetate / 18 h

2: 815 mg / Et₃N / CH₂Cl₂ / -35 °C

With hydrogen; triethylamine; palladium on activated charcoal; In dichloromethane; acetic acid; ethyl acetate;
DOI:10.1002/ejoc.200500146