4-(methyl-{4-[methyl-(4-methylamino-benzoyl)-amino]-benzoyl}-amino)-benzoic acid phenyl ester

Base Information

Chemical Name:4-(methyl-{4-[methyl-(4-methylamino-benzoyl)-amino]-benzoyl}-amino)-benzoic acid phenyl ester
CAS No.:857887-73-1
Molecular Formula:C₃₀H₂₇N₃O₄
Molecular Weight:493.562
Hs Code.:

Synonyms:4-(methyl-{4-[methyl-(4-methylamino-benzoyl)-amino]-benzoyl}-amino)-benzoic acid phenyl ester

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Chemical Property of 4-(methyl-{4-[methyl-(4-methylamino-benzoyl)-amino]-benzoyl}-amino)-benzoic acid phenyl ester

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Technology Process of 4-(methyl-{4-[methyl-(4-methylamino-benzoyl)-amino]-benzoyl}-amino)-benzoic acid phenyl ester

There total 8 articles about 4-(methyl-{4-[methyl-(4-methylamino-benzoyl)-amino]-benzoyl}-amino)-benzoic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 857887-66-2
4-[(4-{[4-(benzyloxycarbonyl-methyl-amino)-benzoyl]-methyl-amino}-benzoyl)-methyl-amino]-benzoic acid phenyl ester

: 857887-73-1
4-(methyl-{4-[methyl-(4-methylamino-benzoyl)-amino]-benzoyl}-amino)-benzoic acid phenyl ester

Guidance literature:: With triethylsilane; triethylamine; palladium dichloride; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/ja0455291

Reference yield:

: 10541-83-0,937737-33-2
N-methyl-p-aminobenzoic acid

: 857887-73-1
4-(methyl-{4-[methyl-(4-methylamino-benzoyl)-amino]-benzoyl}-amino)-benzoic acid phenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 77 percent / NaHCO₃ / tetrahydrofuran / 2 h / 20 °C

2: SOCl₂ / 14 h / 20 °C

3: 42.9 g / Et₃N / CH₂Cl₂ / 24 h / 20 °C

4: 89 percent / Et₃SiH; Et₃N; PdCl₂ / CH₂Cl₂ / 4 h / 20 °C

5: Et₃N / CH₂Cl₂ / 24 h / 20 °C

6: 77 percent / Et₃SiH; Et₃N; PdCl₂ / CH₂Cl₂ / 4 h / 20 °C

With triethylsilane; thionyl chloride; sodium hydrogencarbonate; triethylamine; palladium dichloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja0455291

Reference yield:

: 2528-30-5
4-<<(benzyloxy)carbonyl>methylamino>benzoic acid

: 857887-73-1
4-(methyl-{4-[methyl-(4-methylamino-benzoyl)-amino]-benzoyl}-amino)-benzoic acid phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: SOCl₂ / 14 h / 20 °C

2: 42.9 g / Et₃N / CH₂Cl₂ / 24 h / 20 °C

3: 89 percent / Et₃SiH; Et₃N; PdCl₂ / CH₂Cl₂ / 4 h / 20 °C

4: Et₃N / CH₂Cl₂ / 24 h / 20 °C

5: 77 percent / Et₃SiH; Et₃N; PdCl₂ / CH₂Cl₂ / 4 h / 20 °C

With triethylsilane; thionyl chloride; triethylamine; palladium dichloride; In dichloromethane;
DOI:10.1021/ja0455291