1-<4-(2-bromomethyl-4-methoxyphenyl)-3-methoxyphenyl>-2-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>ethane

Base Information

Chemical Name:1-<4-(2-bromomethyl-4-methoxyphenyl)-3-methoxyphenyl>-2-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>ethane
CAS No.:121404-90-8
Molecular Formula:C₃₁H₃₀Br₂O₄
Molecular Weight:626.385
Hs Code.:

Synonyms:1-<4-(2-bromomethyl-4-methoxyphenyl)-3-methoxyphenyl>-2-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>ethane

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Chemical Property of 1-<4-(2-bromomethyl-4-methoxyphenyl)-3-methoxyphenyl>-2-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>ethane

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Technology Process of 1-<4-(2-bromomethyl-4-methoxyphenyl)-3-methoxyphenyl>-2-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>ethane

There total 19 articles about 1-<4-(2-bromomethyl-4-methoxyphenyl)-3-methoxyphenyl>-2-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 121404-89-5
1-<4-(2-hydroxymethyl-4-methoxyphenyl)-3-methoxyphenyl>-2-<3-(4-hydroxymethylphenoxy)-4-methoxyphenyl>ethane

: 121404-90-8
1-<4-(2-bromomethyl-4-methoxyphenyl)-3-methoxyphenyl>-2-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>ethane

Guidance literature:: With phosphorus tribromide; In benzene; at 80 ℃;

Reference yield:

: 121404-84-0
4-iodo-3-(2-iodo-5-methoxybenzoyloxy)benzaldehyde

: 121404-90-8
1-<4-(2-bromomethyl-4-methoxyphenyl)-3-methoxyphenyl>-2-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>ethane

Guidance literature:: Multi-step reaction with 5 steps

1: 20 percent / Ni(O)(Ph₃P)4

4: LiAlH₄ / tetrahydrofuran

5: PBr₃ / benzene

With lithium aluminium tetrahydride; Ni(O)(Ph₃P)4; phosphorus tribromide; In tetrahydrofuran; benzene;
DOI:10.1016/S0040-4039(00)80674-7

Reference yield:

: 121404-87-3
4-{2-Methoxy-5-[(E)-2-(8-methoxy-6-oxo-6H-benzo[c]chromen-3-yl)-vinyl]-phenoxy}-benzoic acid methyl ester

: 121404-90-8
1-<4-(2-bromomethyl-4-methoxyphenyl)-3-methoxyphenyl>-2-<3-(4-bromomethylphenoxy)-4-methoxyphenyl>ethane

Guidance literature:: Multi-step reaction with 3 steps

2: LiAlH₄ / tetrahydrofuran

3: PBr₃ / benzene

With lithium aluminium tetrahydride; phosphorus tribromide; In tetrahydrofuran; benzene;
DOI:10.1016/S0040-4039(00)80674-7