1,3-di-O-benzyl-2-azido-2-deoxy-4,6-O-methylidene-5-O-(4-methoxybenzyl)-neo-inositol

Base Information

Chemical Name:1,3-di-O-benzyl-2-azido-2-deoxy-4,6-O-methylidene-5-O-(4-methoxybenzyl)-neo-inositol
CAS No.:1380085-02-8
Molecular Formula:C₂₉H₃₁N₃O₆
Molecular Weight:517.582
Hs Code.:

Synonyms:1,3-di-O-benzyl-2-azido-2-deoxy-4,6-O-methylidene-5-O-(4-methoxybenzyl)-neo-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-di-O-benzyl-2-azido-2-deoxy-4,6-O-methylidene-5-O-(4-methoxybenzyl)-neo-inositol

Chemical Property:

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Technology Process of 1,3-di-O-benzyl-2-azido-2-deoxy-4,6-O-methylidene-5-O-(4-methoxybenzyl)-neo-inositol

There total 11 articles about 1,3-di-O-benzyl-2-azido-2-deoxy-4,6-O-methylidene-5-O-(4-methoxybenzyl)-neo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1380085-00-6
C₃₀H₃₁F₃O₉S

: 1380085-02-8
1,3-di-O-benzyl-2-azido-2-deoxy-4,6-O-methylidene-5-O-(4-methoxybenzyl)-neo-inositol

Guidance literature:: With sodium azide; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 20 ℃; for 12h;
DOI:10.1021/jo300444b

Reference yield:

: 1380085-00-6
C₃₀H₃₁F₃O₉S

: 1380085-02-8
1,3-di-O-benzyl-2-azido-2-deoxy-4,6-O-methylidene-5-O-(4-methoxybenzyl)-neo-inositol

: 1380099-47-7
C₂₉H₃₁N₃O₆

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 100 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo300444b

Reference yield:

: 4,6-di-O-benzyl-2-O-(p-methoxybenzyl)-myo-inositol-1,3,5-O-orthoformate

: 1380085-02-8
1,3-di-O-benzyl-2-azido-2-deoxy-4,6-O-methylidene-5-O-(4-methoxybenzyl)-neo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / dichloromethane; toluene / 3 h / 0 - 20 °C

2: pyridine / dichloromethane / 1.25 h / -10 - 20 °C

3: sodium azide / N,N,N,N,N,N-hexamethylphosphoric triamide / 12 h / 20 °C

With pyridine; sodium azide; diisobutylaluminium hydride; In N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; toluene;
DOI:10.1021/jo300444b