Technology Process of C34H31N3O
There total 7 articles about C34H31N3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C34H29N3O2;
With
lithium aluminium tetrahydride;
In
tetrahydrofuran; diethyl ether;
at 20 ℃;
for 13h;
With
methanol; water;
In
tetrahydrofuran; diethyl ether;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: diethyl ether; dichloromethane / 0.5 h / -20 °C
1.2: 1 h / -20 - 20 °C
1.3: 20 °C
2.1: methanesulfonyl chloride; triethylamine / dichloromethane
2.2: 2 h / 65 °C
3.1: copper diacetate / tetrahydrofuran; dichloromethane / 0.25 h / 20 °C
3.2: 0.58 h / 20 °C
4.1: triethylamine / dichloromethane / 12 h / 20 °C
5.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 13 h / 20 °C
With
lithium aluminium tetrahydride; copper diacetate; methanesulfonyl chloride; triethylamine;
In
tetrahydrofuran; diethyl ether; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: formic acid / 2 h / 90 °C
2.1: diethyl ether; dichloromethane / 0.5 h / -20 °C
2.2: 1 h / -20 - 20 °C
2.3: 20 °C
3.1: methanesulfonyl chloride; triethylamine / dichloromethane
3.2: 2 h / 65 °C
4.1: copper diacetate / tetrahydrofuran; dichloromethane / 0.25 h / 20 °C
4.2: 0.58 h / 20 °C
5.1: triethylamine / dichloromethane / 12 h / 20 °C
6.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 13 h / 20 °C
With
lithium aluminium tetrahydride; formic acid; copper diacetate; methanesulfonyl chloride; triethylamine;
In
tetrahydrofuran; diethyl ether; dichloromethane;
