5-methyl-3-(3-methoxyphenyl)-[1,2,3]triazolo[1,5-a][1,4]benzodiazepin-6(4H)-one

Base Information

• Chemical Name: 5-methyl-3-(3-methoxyphenyl)-[1,2,3]triazolo[1,5-a][1,4]benzodiazepin-6(4H)-one
• CAS No.: 1257427-36-3
• Molecular Formula: C₁₈H₁₆N₄O₂
• Molecular Weight: 320.351

Synonyms:5-methyl-3-(3-methoxyphenyl)-[1,2,3]triazolo[1,5-a][1,4]benzodiazepin-6(4H)-one

Chemical Property of 5-methyl-3-(3-methoxyphenyl)-[1,2,3]triazolo[1,5-a][1,4]benzodiazepin-6(4H)-one

Chemical Property:

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Technology Process of 5-methyl-3-(3-methoxyphenyl)-[1,2,3]triazolo[1,5-a][1,4]benzodiazepin-6(4H)-one

There total 1 articles about 5-methyl-3-(3-methoxyphenyl)-[1,2,3]triazolo[1,5-a][1,4]benzodiazepin-6(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-amino-N-methyl-N-[3-(3-methoxyphenyl)prop-2-ynyl]benzamide (1257427-24-9) → 5-methyl-3-(3-methoxyphenyl)-[1,2,3]triazolo[1,5-a][1,4]benzodiazepin-6(4H)-one (1257427-36-3)

Guidance literature:

2-amino-N-methyl-N-[3-(3-methoxyphenyl)prop-2-ynyl]benzamide; With hydrogenchloride; sodium nitrite; In water; at 0 - 3 ℃; for 1.08333h;

With sodium azide; In water; at 100 ℃; for 1.83333h; Cooling with ice;

DOI:10.1039/c0ob00217h

Reference yield: 66.0%

5-methyl-3-(3-methoxyphenyl)-[1,2,3]triazolo[1,5-a][1,4]benzodiazepin-6(4H)-one (1257427-36-3) → 5-methyl-3-(3-methoxyphenyl)-(4H)-[1,2,3]triazolo[1,5-a][1,4]benzodiazepine (1257427-50-1)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Reflux; Inert atmosphere;

DOI:10.1039/c0ob00217h

upstream raw materials:

2-amino-N-methyl-N-[3-(3-methoxyphenyl)prop-2-ynyl]benzamide

Downstream raw materials:

5-methyl-3-(3-methoxyphenyl)-(4H)-[1,2,3]triazolo[1,5-a][1,4]benzodiazepine

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