1-biphenyl-4-yl-2-(5-methoxy-1⁽³⁾H-benzoimidazol-2-ylsulfanyl)-ethanone

Base Information

• Chemical Name: 1-biphenyl-4-yl-2-(5-methoxy-1⁽³⁾H-benzoimidazol-2-ylsulfanyl)-ethanone
• CAS No.: 37052-84-9
• Molecular Formula: C₂₂H₁₈N₂O₂S
• Molecular Weight: 374.463

Synonyms:1-biphenyl-4-yl-2-(5-methoxy-1⁽³⁾H-benzoimidazol-2-ylsulfanyl)-ethanone

Chemical Property of 1-biphenyl-4-yl-2-(5-methoxy-1⁽³⁾H-benzoimidazol-2-ylsulfanyl)-ethanone

Chemical Property:

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Technology Process of 1-biphenyl-4-yl-2-(5-methoxy-1⁽³⁾H-benzoimidazol-2-ylsulfanyl)-ethanone

There total 2 articles about 1-biphenyl-4-yl-2-(5-methoxy-1⁽³⁾H-benzoimidazol-2-ylsulfanyl)-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

2-Bromo-4'-phenylacetophenone (135-73-9) + 6-methoxy-1H-benzoimidazole-2-thiol (37052-78-1) → 1-biphenyl-4-yl-2-(5-methoxy-1(3)H-benzoimidazol-2-ylsulfanyl)-ethanone (37052-84-9)

Guidance literature:

With potassium carbonate; In acetone; Reflux;

DOI:10.1134/S1070428021060130

Reference yield:

→ 1-biphenyl-4-yl-2-(5-methoxy-1(3)H-benzoimidazol-2-ylsulfanyl)-ethanone (37052-84-9)

Guidance literature:

Thioalkohol (II), p-Phenyl-phenacylbromid;

Reference yield: 71.0%

C6H6F2N2O2S + 1-biphenyl-4-yl-2-(5-methoxy-1(3)H-benzoimidazol-2-ylsulfanyl)-ethanone (37052-84-9) → N’-(1-([1,1'-biphenyl]-4-yl)-2-((6-methoxy-1H-benzo[d]imidazol-2-yl)thio)ethylidene)-2,4-difluorobenzenesulfonohydrazide

Guidance literature:

With acetic acid; In methanol; for 4h; Reflux;

DOI:10.1016/j.molstruc.2021.130029

upstream raw materials:

2-Bromo-4'-phenylacetophenone

6-methoxy-1H-benzoimidazole-2-thiol

Downstream raw materials:

3-biphenyl-4-yl-6-methoxy-benzo[4,5]imidazo[2,1-b]thiazole

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