4-benzyl-5-phenylhex-5-enal

Base Information

Chemical Name:4-benzyl-5-phenylhex-5-enal
CAS No.:1300035-57-7
Molecular Formula:C₁₉H₂₀O
Molecular Weight:264.367
Hs Code.:

Synonyms:4-benzyl-5-phenylhex-5-enal

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Chemical Property of 4-benzyl-5-phenylhex-5-enal

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Technology Process of 4-benzyl-5-phenylhex-5-enal

There total 7 articles about 4-benzyl-5-phenylhex-5-enal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1300035-65-7
4-benzyl-5-phenylhex-5-en-1-ol

: 1300035-57-7
4-benzyl-5-phenylhex-5-enal

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol200725m

Reference yield:

: 1300035-52-2
2-benzyl-5-(tert-butyldimethylsilanyloxy)pentanoic acid methoxymethylamide

: 1300035-57-7
4-benzyl-5-phenylhex-5-enal

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / 25 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

4.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 2 h / -78 - 20 °C / Inert atmosphere

With n-butyllithium; oxalyl dichloride; tetrabutyl ammonium fluoride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; hexane; dichloromethane; 4.1: Swern oxidation;
DOI:10.1021/ol200725m

Reference yield:

: 542-28-9,26354-94-9
3,4,5,6-tetrahydro-2H-pyran-2-one

: 1300035-57-7
4-benzyl-5-phenylhex-5-enal

Guidance literature:: Multi-step reaction with 7 steps

1.1: trimethylaluminum / dichloromethane; toluene / 0.33 h / 0 °C / Inert atmosphere

1.2: Inert atmosphere

1.3: 1 h / 0 °C / Inert atmosphere

2.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

3.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: tetrahydrofuran / 25 h / 0 - 20 °C / Inert atmosphere

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C / Inert atmosphere

5.2: 0 - 20 °C / Inert atmosphere

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

7.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 2 h / -78 - 20 °C / Inert atmosphere

With dmap; n-butyllithium; oxalyl dichloride; tetrabutyl ammonium fluoride; trimethylaluminum; dimethyl sulfoxide; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; toluene; 7.1: Swern oxidation;
DOI:10.1021/ol200725m