1,2-dicarba-closo-dodecaborane-9-diphenylphosphinomethyl oxide

Base Information

Chemical Name:1,2-dicarba-closo-dodecaborane-9-diphenylphosphinomethyl oxide
CAS No.:1228071-14-4
Molecular Formula:C₁₅H₂₃B₁₀OP
Molecular Weight:358.431
Hs Code.:

Synonyms:1,2-dicarba-closo-dodecaborane-9-diphenylphosphinomethyl oxide

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Chemical Property of 1,2-dicarba-closo-dodecaborane-9-diphenylphosphinomethyl oxide

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Technology Process of 1,2-dicarba-closo-dodecaborane-9-diphenylphosphinomethyl oxide

There total 1 articles about 1,2-dicarba-closo-dodecaborane-9-diphenylphosphinomethyl oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 61654-04-4
o-carborane-9-carboxylic acid

: 7732-18-5
water

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1228071-14-4
1,2-dicarba-closo-dodecaborane-9-diphenylphosphinomethyl oxide

Guidance literature:: In neat (no solvent); (Ar) Ph2PCl was added to cooled (0°C) mixt. C2B10H11COOH and H2O,heated for 3 h at 80°C and for 80 h at 180°C; react. mixt. was cooled, product was triturated with toluene, heated to 80°C, ppt. was filtered off, washed with 5% aq. soln. Na2CO3, dried, recrystd. from MeCN;
DOI:10.1007/s11172-008-0326-y

Reference yield: 98.0%

: 1228071-14-4
1,2-dicarba-closo-dodecaborane-9-diphenylphosphinomethyl oxide

: 1228071-11-1
9-diphenylphosphinomethyl-1,2-dicarba-closo-dodecaborane

Guidance literature:: With trichlorosilane; In toluene; (Ar) HSiCl3 was added to suspn. C2B10H11(CH2PO(C6H5)2) in toluene, heated for 5 h at 100°C; react. mixt. was cooled, concd. in vac., recrystd. from heptane-toluene;elem. anal.;
DOI:10.1007/s11172-008-0326-y