(2S)-3-[[1-[3-[1,3-bis(tert-butoxycarbonyl)hexahydropyrimidin-2-ylidene]aminophenyl]piperidin-4-yl]carbonylamino]-2-(benzyloxycarbonylamino)propanoic acid methyl ester

Base Information

• Chemical Name: (2S)-3-[[1-[3-[1,3-bis(tert-butoxycarbonyl)hexahydropyrimidin-2-ylidene]aminophenyl]piperidin-4-yl]carbonylamino]-2-(benzyloxycarbonylamino)propanoic acid methyl ester
• CAS No.: 461719-88-0
• Molecular Formula: C₂₄H₃₀N₄O₅
• Molecular Weight: 454.526

Synonyms:(2S)-3-[[1-[3-[1,3-bis(tert-butoxycarbonyl)hexahydropyrimidin-2-ylidene]aminophenyl]piperidin-4-yl]carbonylamino]-2-(benzyloxycarbonylamino)propanoic acid methyl ester

Chemical Property of (2S)-3-[[1-[3-[1,3-bis(tert-butoxycarbonyl)hexahydropyrimidin-2-ylidene]aminophenyl]piperidin-4-yl]carbonylamino]-2-(benzyloxycarbonylamino)propanoic acid methyl ester

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Technology Process of (2S)-3-[[1-[3-[1,3-bis(tert-butoxycarbonyl)hexahydropyrimidin-2-ylidene]aminophenyl]piperidin-4-yl]carbonylamino]-2-(benzyloxycarbonylamino)propanoic acid methyl ester

There total 1 articles about (2S)-3-[[1-[3-[1,3-bis(tert-butoxycarbonyl)hexahydropyrimidin-2-ylidene]aminophenyl]piperidin-4-yl]carbonylamino]-2-(benzyloxycarbonylamino)propanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2S)-2-benzyloxycarbonylamino-3-[[1-(3-nitrophenyl)-piperidin-4-yl]carbonylamino]propanoic acid methyl ester (461719-87-9) → (2S)-3-[[1-[3-[1,3-bis(tert-butoxycarbonyl)hexahydropyrimidin-2-ylidene]aminophenyl]piperidin-4-yl]carbonylamino]-2-(benzyloxycarbonylamino)propanoic acid methyl ester (461719-88-0)

Guidance literature:

With iron; ammonium chloride; In ethanol; water; at 90 ℃; for 4h;

Reference yield:

(2S)-3-[[1-[3-[1,3-bis(tert-butoxycarbonyl)hexahydropyrimidin-2-ylidene]aminophenyl]piperidin-4-yl]carbonylamino]-2-(benzyloxycarbonylamino)propanoic acid methyl ester (461719-88-0) → (2S)-2-benzyloxycarbonylamino-3-[[1-(3-cyclic guanidinophenyl)piperidin-4-yl]carbonylamino]-propanoic acid methyl ester

Guidance literature:

With Benzyl isothiocyanate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 25 ℃;

Reference yield:

1,3-bis(tert-butoxycarbonyl)-2(1H)-tetrahydropyrimidinethione + (2S)-3-[[1-[3-[1,3-bis(tert-butoxycarbonyl)hexahydropyrimidin-2-ylidene]aminophenyl]piperidin-4-yl]carbonylamino]-2-(benzyloxycarbonylamino)propanoic acid methyl ester (461719-88-0) → (2S)-3-[[1-[3-[1,3-bis(tert-butoxycarbonyl)hexahydropyrimidin-2-ylidene]aminophenyl]piperidin-4-yl]carbonylamino]-2-(benzyloxycarbonylamino)propanoic acid methyl ester (461719-89-1)

Guidance literature:

With triethylamine; mercury dichloride; In N,N-dimethyl-formamide; at 25 ℃;

upstream raw materials:

(2S)-2-benzyloxycarbonylamino-3-[[1-(3-nitrophenyl)-piperidin-4-yl]carbonylamino]propanoic acid methyl ester

Downstream raw materials:

(2S)-3-[[1-[3-[1,3-bis(tert-butoxycarbonyl)hexahydropyrimidin-2-ylidene]aminophenyl]piperidin-4-yl]carbonylamino]-2-(benzyloxycarbonylamino)propanoic acid methyl ester

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