1-Phenyl-5-aminotetrazole

Base Information

• Chemical Name: 1-Phenyl-5-aminotetrazole
• CAS No.: 5855-52-7
• Molecular Formula: C15H12N2
• Molecular Weight: 220.274
• Hs Code.: 2933499090
• Mol file: 5855-52-7.mol

Synonyms:2-Phenyl-4-quinolinamine;2-Phenyl-quinolin-4-ylamine;4-Quinolinamine, 2-phenyl-;4-amino-2-phenylquinoline;4-Quinolinamine,2-phenyl;Quinoline,4-amino-2-phenyl;2-Phenyl-4-aminoquinoline;

Chemical Property of 1-Phenyl-5-aminotetrazole

Chemical Property:

• Vapor Pressure: 3.56E-08mmHg at 25°C
• Boiling Point: 446.7°Cat760mmHg
• Flash Point: 254.4°C
• PSA: 38.91000
• Density: 1.194g/cm³
• LogP: 4.06520
• Storage Temp.: 2-8°C

Purity/Quality:

2-phenylquinolin-4-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Phenyl-5-aminotetrazole

There total 39 articles about 1-Phenyl-5-aminotetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4-chloro-2-phenylquinoline (4979-79-7) → 2-phenylquinolin-4-amine (5855-52-7)

Guidance literature:

4-chloro-2-phenylquinoline; With phenol; at 180 ℃; for 1h;

With ammonia; at 180 ℃; for 5h;

With sodium hydroxide; In water; at 20 ℃;

DOI:10.1016/j.bmc.2010.01.061

Reference yield: 94.0%

4-(1,1,1,3,3,3-Hexamethyl-disilazan-2-yl)-2-phenyl-quinoline (189877-75-6) → 2-phenylquinolin-4-amine (5855-52-7)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 23 ℃; for 2h;

DOI:10.1021/jo970101o

Reference yield: 89.0%

4-nitro-2-phenylquinoline (155057-20-8) → 2-phenylquinolin-4-amine (5855-52-7)

Guidance literature:

With palladium on activated charcoal; ammonium formate; In methanol; for 4h;

DOI:10.1055/s-0036-1588147

upstream raw materials:

2-Phenylquinoline

2-phenyl-4-quinolinol

2-phenyl quinoline-4-carboxamide

2-thienyl lithium

Downstream raw materials:

N-(2-phenyl-[4]quinolyl)-glycine

N-(2-phenyl-quinolin-4-yl)-acetamide

N-(2-phenyl-[4]quinolyl)-acetoacetamide