4-(decyloxy)biphenyl 1-(4-methoxyphenyl)-1H-1,2,3-triazole-4-carboxylate

Base Information

Chemical Name:4-(decyloxy)biphenyl 1-(4-methoxyphenyl)-1H-1,2,3-triazole-4-carboxylate
CAS No.:1422423-76-4
Molecular Formula:C₃₂H₃₇N₃O₄
Molecular Weight:527.663
Hs Code.:

Synonyms:4-(decyloxy)biphenyl 1-(4-methoxyphenyl)-1H-1,2,3-triazole-4-carboxylate

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Chemical Property of 4-(decyloxy)biphenyl 1-(4-methoxyphenyl)-1H-1,2,3-triazole-4-carboxylate

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Technology Process of 4-(decyloxy)biphenyl 1-(4-methoxyphenyl)-1H-1,2,3-triazole-4-carboxylate

There total 5 articles about 4-(decyloxy)biphenyl 1-(4-methoxyphenyl)-1H-1,2,3-triazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 91577-95-6
4-hydroxy-4'-decyloxybiphenyl

: 1-(4-Methoxy-phenyl)-1H-[1,2,3]triazole-4-carbonyl chloride

: 1422423-76-4
4-(decyloxy)biphenyl 1-(4-methoxyphenyl)-1H-1,2,3-triazole-4-carboxylate

Guidance literature:: With triethylamine; In dichloromethane; for 48h; Reflux; Cooling with ice; Inert atmosphere;
DOI:10.1016/j.molstruc.2012.09.020

Reference yield:

: 4916-13-6
1-(4-methoxyphenyl)-1H-[1,2,3]-triazolyl-4-carboxylic acid

: 1422423-76-4
4-(decyloxy)biphenyl 1-(4-methoxyphenyl)-1H-1,2,3-triazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 85 °C / Inert atmosphere

2: triethylamine / dichloromethane / 48 h / Reflux; Cooling with ice; Inert atmosphere

With thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/j.molstruc.2012.09.020

Reference yield:

: 92-88-6
4,4'-Dihydroxybiphenyl

: 1422423-76-4
4-(decyloxy)biphenyl 1-(4-methoxyphenyl)-1H-1,2,3-triazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / dimethyl sulfoxide / 24 h

2: triethylamine / dichloromethane / 48 h / Reflux; Cooling with ice; Inert atmosphere

With triethylamine; potassium hydroxide; In dichloromethane; dimethyl sulfoxide;
DOI:10.1016/j.molstruc.2012.09.020