2-(N-tert-butyloxycarbonyl-N-methyl-amino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]-acetic acid amide

Base Information

Chemical Name:2-(N-tert-butyloxycarbonyl-N-methyl-amino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]-acetic acid amide
CAS No.:276681-98-2
Molecular Formula:C₂₂H₂₉N₃O₅S
Molecular Weight:447.555
Hs Code.:

Synonyms:2-(N-tert-butyloxycarbonyl-N-methyl-amino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]-acetic acid amide

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Chemical Property of 2-(N-tert-butyloxycarbonyl-N-methyl-amino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]-acetic acid amide

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Technology Process of 2-(N-tert-butyloxycarbonyl-N-methyl-amino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]-acetic acid amide

There total 1 articles about 2-(N-tert-butyloxycarbonyl-N-methyl-amino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]-acetic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 13734-36-6
N-(tert-butoxycarbonyl)sarcosine

: 244013-66-9
3-amino-N-(2,3-dimethylphenylbenzene sulphonamide)

: 276681-98-2
2-(N-tert-butyloxycarbonyl-N-methyl-amino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]-acetic acid amide

Guidance literature:: With 4-methyl-morpholine; isobutyl chloroformate; In N,N-dimethyl-formamide; at -15 - 20 ℃;
DOI:10.1211/146080800128735746

Reference yield:

: 276681-98-2
2-(N-tert-butyloxycarbonyl-N-methyl-amino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]-acetic acid amide

: N-[3-(2,3-dimethyl-phenylsulfamoyl)-phenyl]-2-methylamino-acetamide

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;
DOI:10.1211/146080800128735746

Reference yield:

: 276681-98-2
2-(N-tert-butyloxycarbonyl-N-methyl-amino)-N-[3-(2,3-dimethylphenylaminosulphonyl)phenyl]-acetic acid amide

: N-{[3-(2,3-dimethylphenylaminosulphonyl)phenylaminocarbonyl]methyl}-N-methylheptadecanoic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: HCl (gas) / dioxane / 2 h / 20 °C

2: 46 percent / N-methylmorpholine; isobutyl chloroformate / dimethylformamide / -15 - 20 °C

With 4-methyl-morpholine; hydrogenchloride; isobutyl chloroformate; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1211/146080800128735746