C₁₈H₃₂O₅Si

Base Information

Chemical Name:C₁₈H₃₂O₅Si
CAS No.:945468-66-6
Molecular Formula:C₁₈H₃₂O₅Si
Molecular Weight:356.535
Hs Code.:

C<sub>18</sub>H<sub>32</sub>O<sub>5</sub>Si

Synonyms:C₁₈H₃₂O₅Si

Suppliers and Price of C₁₈H₃₂O₅Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₈H₃₂O₅Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₈H₃₂O₅Si

There total 8 articles about C₁₈H₃₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 945468-65-5
C₂₁H₄₀O₅Si₂

: 945468-66-6
C₁₈H₃₂O₅Si

Guidance literature:: With potassium carbonate; In methanol; at 23 ℃; for 0.025h;
DOI:10.1016/j.tetlet.2007.04.136

Reference yield:

: 945468-62-2
C₁₄H₂₀O₃

: 945468-66-6
C₁₈H₃₂O₅Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: OsO₄; NMO / dioxane / 1 h / 23 °C / pH 7

1.2: 68 percent / NaIO₄ / dioxane / 3 h

2.1: 99 percent / NaH / tetrahydrofuran / 12.5 h / 23 °C

3.1: 73 percent / DIBALH / CH₂Cl₂ / 0.67 h / -78 °C

4.1: (+)-diisopropyl tartrate; Ti(OiPr)4; TBHP / 4A MS / CH₂Cl₂ / 12 h / -30 °C

5.1: 100 percent / LiAlH₄ / tetrahydrofuran / 1 h / 24 °C

6.1: 95 percent / 2,6-lutidine / CH₂Cl₂ / 0.75 h / -40 °C

7.1: 89 percent / K₂CO₃ / methanol / 0.03 h / 23 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; osmium(VIII) oxide; lithium aluminium tetrahydride; N-methyl-2-indolinone; L-(+)-diisopropyl tartrate; sodium hydride; diisobutylaluminium hydride; potassium carbonate; 4A MS; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; 2.1: Horner-Wadsworth-Emmons reaction / 4.1: Katsuki-Sharpless asymmetric epoxidation;
DOI:10.1016/j.tetlet.2007.04.136

Reference yield:

: C₁₇H₂₄O₅

: 945468-66-6
C₁₈H₃₂O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1: 73 percent / DIBALH / CH₂Cl₂ / 0.67 h / -78 °C

2: (+)-diisopropyl tartrate; Ti(OiPr)4; TBHP / 4A MS / CH₂Cl₂ / 12 h / -30 °C

3: 100 percent / LiAlH₄ / tetrahydrofuran / 1 h / 24 °C

4: 95 percent / 2,6-lutidine / CH₂Cl₂ / 0.75 h / -40 °C

5: 89 percent / K₂CO₃ / methanol / 0.03 h / 23 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; lithium aluminium tetrahydride; L-(+)-diisopropyl tartrate; diisobutylaluminium hydride; potassium carbonate; 4A MS; In tetrahydrofuran; methanol; dichloromethane; 2: Katsuki-Sharpless asymmetric epoxidation;
DOI:10.1016/j.tetlet.2007.04.136