3-Chloro-1-(4-methoxy-phenyl)-4-((E)-1-methyl-2-phenyl-vinyl)-3-phenylsulfanyl-azetidin-2-one

Base Information

• Chemical Name: 3-Chloro-1-(4-methoxy-phenyl)-4-((E)-1-methyl-2-phenyl-vinyl)-3-phenylsulfanyl-azetidin-2-one
• CAS No.: 94612-30-3
• Molecular Formula: C₂₅H₂₂ClNO₂S
• Molecular Weight: 435.974

Synonyms:3-Chloro-1-(4-methoxy-phenyl)-4-((E)-1-methyl-2-phenyl-vinyl)-3-phenylsulfanyl-azetidin-2-one

Chemical Property of 3-Chloro-1-(4-methoxy-phenyl)-4-((E)-1-methyl-2-phenyl-vinyl)-3-phenylsulfanyl-azetidin-2-one

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Technology Process of 3-Chloro-1-(4-methoxy-phenyl)-4-((E)-1-methyl-2-phenyl-vinyl)-3-phenylsulfanyl-azetidin-2-one

There total 5 articles about 3-Chloro-1-(4-methoxy-phenyl)-4-((E)-1-methyl-2-phenyl-vinyl)-3-phenylsulfanyl-azetidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

13e (94612-52-9,101628-75-5,123670-05-3) → 3-Chloro-1-(4-methoxy-phenyl)-4-((E)-1-methyl-2-phenyl-vinyl)-3-phenylsulfanyl-azetidin-2-one (94612-30-3)

Guidance literature:

With sulfuryl dichloride; In dichloromethane; at -10 ℃;

DOI:10.1021/jo00285a023

Reference yield:

1-(4-Methoxy-phenyl)-4-((E)-1-methyl-2-phenyl-vinyl)-3-phenylsulfanyl-azetidin-2-one (94612-52-9,101628-75-5,123670-05-3) → 3-Chloro-1-(4-methoxy-phenyl)-4-((E)-1-methyl-2-phenyl-vinyl)-3-phenylsulfanyl-azetidin-2-one (94612-30-3)

Guidance literature:

With sulfuryl dichloride; In dichloromethane; at 0 ℃;

DOI:10.1016/S0040-4039(01)81505-7

Reference yield:

phenylthioglicolic acid potassium salt (84900-63-0) → 3-Chloro-1-(4-methoxy-phenyl)-4-((E)-1-methyl-2-phenyl-vinyl)-3-phenylsulfanyl-azetidin-2-one (94612-30-3)

Guidance literature:

Multi-step reaction with 2 steps

1: (C₂H₅)3N, cyanuric chloride

2: sulfuryl chloride / CH₂Cl₂ / 0 °C

With sulfuryl dichloride; 1,3,5-trichloro-2,4,6-triazine; triethylamine; In dichloromethane;

DOI:10.1016/S0040-4039(01)81505-7

upstream raw materials:

13e

1-(4-Methoxy-phenyl)-4-((E)-1-methyl-2-phenyl-vinyl)-3-phenylsulfanyl-azetidin-2-one

phenylthioglicolic acid potassium salt

(4-Methoxy-phenyl)-[(E)-2-methyl-3-phenyl-prop-2-en-(Z)-ylidene]-amine

Downstream raw materials:

(3S,4R)-3-Methoxy-1-(4-methoxy-phenyl)-4-((E)-1-methyl-2-phenyl-vinyl)-3-phenylsulfanyl-azetidin-2-one

1-(4-methoxyphenyl)-4-(3-phenylprop-2-en-2-yl)-2,3-azetidinedione

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