N-(5-chloropyridine-2-yl)-2-[(4-ethaneimidoyl-methylaminophenylcarbonyl)amino]benzamide

Base Information

Chemical Name:N-(5-chloropyridine-2-yl)-2-[(4-ethaneimidoyl-methylaminophenylcarbonyl)amino]benzamide
CAS No.:1333126-79-6
Molecular Formula:C₂₂H₂₀ClN₅O₂
Molecular Weight:421.886
Hs Code.:

Synonyms:N-(5-chloropyridine-2-yl)-2-[(4-ethaneimidoyl-methylaminophenylcarbonyl)amino]benzamide

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Chemical Property of N-(5-chloropyridine-2-yl)-2-[(4-ethaneimidoyl-methylaminophenylcarbonyl)amino]benzamide

Chemical Property:

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Technology Process of N-(5-chloropyridine-2-yl)-2-[(4-ethaneimidoyl-methylaminophenylcarbonyl)amino]benzamide

There total 8 articles about N-(5-chloropyridine-2-yl)-2-[(4-ethaneimidoyl-methylaminophenylcarbonyl)amino]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1333127-00-6
N-(5-chloropyridine-2-yl)-2-[(4-methylaminophenylcarbonyl)amino]benzamide

: 75-05-8,26809-02-9
acetonitrile

: 1333126-79-6
N-(5-chloropyridine-2-yl)-2-[(4-ethaneimidoyl-methylaminophenylcarbonyl)amino]benzamide

Guidance literature:: N-(5-chloropyridine-2-yl)-2-[(4-methylaminophenylcarbonyl)amino]benzamide; acetonitrile; With hydrogenchloride; at 5 ℃; for 48.5h; Cooling with ice;

With sodium hydrogencarbonate; In acetonitrile;

Reference yield:

: 552-16-9,104810-18-6
ortho-nitrobenzoic acid

: 1333126-79-6
N-(5-chloropyridine-2-yl)-2-[(4-ethaneimidoyl-methylaminophenylcarbonyl)amino]benzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / 4 h

1.2: 15 h

2.1: hydrogenchloride; tin(ll) chloride / ethyl acetate; water / Reflux

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 72 h

4.1: isopropyl alcohol; sodium hydroxide / 3 h

5.1: hydrogenchloride / 48.5 h / 5 °C / Cooling with ice

With hydrogenchloride; thionyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; isopropyl alcohol; tin(ll) chloride; sodium hydroxide; In tetrahydrofuran; water; ethyl acetate;

Reference yield:

: 280771-60-0
N-(5-chloropyridine-2-yl)-2-nitrobenzamide

: 1333126-79-6
N-(5-chloropyridine-2-yl)-2-[(4-ethaneimidoyl-methylaminophenylcarbonyl)amino]benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride; tin(ll) chloride / ethyl acetate; water / Reflux

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 72 h

3: isopropyl alcohol; sodium hydroxide / 3 h

4: hydrogenchloride / 48.5 h / 5 °C / Cooling with ice

With hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; isopropyl alcohol; tin(ll) chloride; sodium hydroxide; In tetrahydrofuran; water; ethyl acetate;