C₁₇H₂₀O₃

Base Information

• Chemical Name: C₁₇H₂₀O₃
• CAS No.: 130147-87-4
• Molecular Formula: C₁₇H₂₀O₃
• Molecular Weight: 272.344
• Mol file: 130147-87-4.mol

Synonyms:C₁₇H₂₀O₃

Chemical Property of C₁₇H₂₀O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₀O₃

There total 5 articles about C₁₇H₂₀O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

6-Bromo-2-(2-hydroxy-3-hydroxymethyl-5-methyl-benzyl)-3,4-dimethyl-phenol (149385-41-1) → C17H20O3 (130147-87-4)

Guidance literature:

With potassium hydroxide; hydrogen; nickel; In methanol; under 760 Torr; Ambient temperature;

DOI:10.1021/jo00067a040

Reference yield:

3,4-Dimethylphenol (95-65-8) → C17H20O3 (130147-87-4)

Guidance literature:

Multi-step reaction with 5 steps

1: 76 percent / bromine / CHCl₃ / 1 h / 5 °C

2: 49 percent / HBr gas / acetic acid / 0.33 h

3: 69 percent / CH₂Cl₂ / 5 h / 60 °C

4: 72 percent / NaOH / H₂O / Ambient temperature

5: 85 percent / H₂, KOH / Raney nickel / methanol / 760 Torr / Ambient temperature

With potassium hydroxide; sodium hydroxide; hydrogen bromide; hydrogen; bromine; nickel; In methanol; dichloromethane; chloroform; water; acetic acid;

DOI:10.1021/jo00067a040

Reference yield:

6-bromo-2-(bromomethyl)-3,4-dimethylphenol (149385-39-7) → C17H20O3 (130147-87-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 69 percent / CH₂Cl₂ / 5 h / 60 °C

2: 72 percent / NaOH / H₂O / Ambient temperature

3: 85 percent / H₂, KOH / Raney nickel / methanol / 760 Torr / Ambient temperature

With potassium hydroxide; sodium hydroxide; hydrogen; nickel; In methanol; dichloromethane; water;

DOI:10.1021/jo00067a040

upstream raw materials:

6-Bromo-2-(2-hydroxy-3-hydroxymethyl-5-methyl-benzyl)-3,4-dimethyl-phenol

3,4-Dimethylphenol

2-bromo-4,5-dimethylphenol

6-bromo-2-(bromomethyl)-3,4-dimethylphenol