Technology Process of C32H43N3O12
There total 3 articles about C32H43N3O12 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; ascorbic acid;
In
water; N,N-dimethyl-formamide;
at 20 ℃;
for 0.75h;
regioselective reaction;
Inert atmosphere;
DOI:10.1016/j.carres.2012.08.001
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / mineral oil; toluene / 2 h / Reflux; Inert atmosphere
2.1: hydrogenchloride; sodium nitrite / water; acetone / 0 °C
2.2: 5 °C
3.1: copper(ll) sulfate pentahydrate; ascorbic acid / water; N,N-dimethyl-formamide / 0.75 h / 20 °C / Inert atmosphere
With
hydrogenchloride; copper(ll) sulfate pentahydrate; sodium hydride; ascorbic acid; sodium nitrite;
In
water; N,N-dimethyl-formamide; acetone; toluene; mineral oil;
DOI:10.1016/j.carres.2012.08.001
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / mineral oil; toluene / 2 h / Reflux; Inert atmosphere
2.1: hydrogenchloride; sodium nitrite / water; acetone / 0 °C
2.2: 5 °C
3.1: copper(ll) sulfate pentahydrate; ascorbic acid / water; N,N-dimethyl-formamide / 0.75 h / 20 °C / Inert atmosphere
With
hydrogenchloride; copper(ll) sulfate pentahydrate; sodium hydride; ascorbic acid; sodium nitrite;
In
water; N,N-dimethyl-formamide; acetone; toluene; mineral oil;
DOI:10.1016/j.carres.2012.08.001
