triphenylmethyl [(tris(pentafluorophenyl)boran)2 cyanide]

Base Information

• Chemical Name: triphenylmethyl [(tris(pentafluorophenyl)boran)2 cyanide]
• CAS No.: 239805-47-1
• Molecular Formula: C₁₉H₁₅*C₃₇B₂F₃₀N
• Molecular Weight: 1293.32
• Mol file: 239805-47-1.mol

Synonyms:triphenylmethyl [(tris(pentafluorophenyl)boran)2 cyanide]

Chemical Property of triphenylmethyl [(tris(pentafluorophenyl)boran)2 cyanide]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of triphenylmethyl [(tris(pentafluorophenyl)boran)2 cyanide]

There total 4 articles about triphenylmethyl [(tris(pentafluorophenyl)boran)2 cyanide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

potassium cyanide + trityl chloride (76-83-5) + tris(pentafluorophenyl)borane*(diethyl ether) → triphenylmethyl [(tris(pentafluorophenyl)boran)2 cyanide] (239805-47-1)

Guidance literature:

In diethyl ether; dichloromethane; (N2); addn. of Et2O to a mixt. of boron compd. and KCN, stirring overnight, evapn., drying, addn. of triphenylchloromethane, addn. of CH2Cl2, stirring for 1 h; filtration, concn., addn. of light petroleum, cooling to -20°C; elem. anal.;

DOI:10.1021/ja002820h

Reference yield: 45.0%

potassium cyanide (151-50-8) + trityl chloride (76-83-5) + tris(pentafluorophenyl)borane*(diethyl ether) → triphenylmethyl [(tris(pentafluorophenyl)boran)2 cyanide] (239805-47-1)

Guidance literature:

potassium cyanide; tris(pentafluorophenyl)borane*(diethyl ether); In diethyl ether; for 12h;

trityl chloride; In dichloromethane; for 1h; Further stages.;

DOI:10.1021/ja002820h

Reference yield:

tris(pentafluorophenyl)borate (1109-15-5) + potassium cyanide (151-50-8) + trityl chloride (76-83-5) → triphenylmethyl [(tris(pentafluorophenyl)boran)2 cyanide] (239805-47-1)

Guidance literature:

tris(pentafluorophenyl)borate; potassium cyanide; In diethyl ether; at 20 ℃;

trityl chloride; In dichloromethane;

DOI:10.1039/a903788h

upstream raw materials:

tris(pentafluorophenyl)borate

potassium cyanide

trityl chloride

Downstream raw materials:

(C₅H₅)2ZrCH₃(NC)B(C₆F₅)3

(C₅H₃(Si(CH₃)3)2)2ZrCH₃NCB(C₆F₅)3*C₆H₅CH₃