(2-((2-(3,3-dimethylbut-1-yn-1-yl)phenyl)ethynyl)phenyl)-(methyl)sulfane

Base Information

Chemical Name:(2-((2-(3,3-dimethylbut-1-yn-1-yl)phenyl)ethynyl)phenyl)-(methyl)sulfane
CAS No.:1609017-36-8
Molecular Formula:C₂₁H₂₀S
Molecular Weight:304.456
Hs Code.:

Synonyms:(2-((2-(3,3-dimethylbut-1-yn-1-yl)phenyl)ethynyl)phenyl)-(methyl)sulfane

Suppliers and Price of (2-((2-(3,3-dimethylbut-1-yn-1-yl)phenyl)ethynyl)phenyl)-(methyl)sulfane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2-((2-(3,3-dimethylbut-1-yn-1-yl)phenyl)ethynyl)phenyl)-(methyl)sulfane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2-((2-(3,3-dimethylbut-1-yn-1-yl)phenyl)ethynyl)phenyl)-(methyl)sulfane

There total 4 articles about (2-((2-(3,3-dimethylbut-1-yn-1-yl)phenyl)ethynyl)phenyl)-(methyl)sulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 917-92-0
3,3-Dimethylbut-1-yne

: 1609017-33-5
(2-((2-iodophenyl)ethynyl)phenyl)(methyl)sulfane

: 1609017-36-8
(2-((2-(3,3-dimethylbut-1-yn-1-yl)phenyl)ethynyl)phenyl)-(methyl)sulfane

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-butylamine; In diethyl ether; at 20 ℃; for 6h;
DOI:10.1021/jo500377v

Reference yield:

: 78905-08-5
<(o-methylthio)phenyl>acetylene

: 1609017-36-8
(2-((2-(3,3-dimethylbut-1-yn-1-yl)phenyl)ethynyl)phenyl)-(methyl)sulfane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide; N-butylamine / diethyl ether / 6 h / 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide; N-butylamine / diethyl ether / 6 h / 20 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-butylamine; In diethyl ether; 1: |Sonogashira Cross-Coupling / 2: |Sonogashira Cross-Coupling;
DOI:10.1021/jo500377v

Reference yield:

: 415680-02-3
trimethyl{[2-(methylsulfanyl)phenyl]ethynyl}silane

: 1609017-36-8
(2-((2-(3,3-dimethylbut-1-yn-1-yl)phenyl)ethynyl)phenyl)-(methyl)sulfane

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide; N-butylamine / diethyl ether / 6 h / 20 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide; N-butylamine / diethyl ether / 6 h / 20 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; N-butylamine; In tetrahydrofuran; diethyl ether; 2: |Sonogashira Cross-Coupling / 3: |Sonogashira Cross-Coupling;
DOI:10.1021/jo500377v