C₃₆H₄₅NO₄Si

Base Information

Chemical Name:C₃₆H₄₅NO₄Si
CAS No.:880152-39-6
Molecular Formula:C₃₆H₄₅NO₄Si
Molecular Weight:583.843
Hs Code.:

C<sub>36</sub>H<sub>45</sub>NO<sub>4</sub>Si

Synonyms:C₃₆H₄₅NO₄Si

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Chemical Property of C₃₆H₄₅NO₄Si

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Technology Process of C₃₆H₄₅NO₄Si

There total 16 articles about C₃₆H₄₅NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 880152-44-3
C₃₆H₄₄ClNO₄Si

: 880152-39-6
C₃₆H₄₅NO₄Si

Guidance literature:: With acetic acid; zinc; at 20 ℃; for 2h;
DOI:10.1021/ol053059p

Reference yield:

: 880152-30-7
2-(3-tert-butoxycarbonylamino-4-hydroxy-butyl)-cyclohex-1-enecarboxylic acid ethyl ester

: 880152-39-6
C₃₆H₄₅NO₄Si

Guidance literature:: Multi-step reaction with 11 steps

1: imidazole / CH₂Cl₂ / 20 °C

2: 12.0 g / DIBAL-H / CH₂Cl₂ / -78 - 0 °C

3: pyridine / 20 °C

4: 100 percent / TFA / CH₂Cl₂ / 1 h / 0 °C

5: 61 percent / pyridine / ethanol / 48 h / Heating

6: K₂CO₃ / methanol; H₂O / 1 h / 20 °C

7: 504.0 mg / N-methylmorpholine-N-oxide; TPAP; 4 Angstroem molecular sieves / CH₂Cl₂ / 1 h / 20 °C

8: 68 percent / Na₂SO₄; piperidinium acetate / ethyl acetate; toluene / Heating

9: 76 percent / N-chlorosuccinimide; H₂O / 2-methyl-propan-2-ol / 1 h / 20 °C

10: 66 percent / N-methylmorpholine-N-oxide; TPAP; 4 Angstroem molecular sieves / CH₂Cl₂ / 4 h / 20 °C

11: 98 percent / Zn; HOAc / 2 h / 20 °C

With pyridine; 1H-imidazole; N-chloro-succinimide; tetrapropylammonium perruthennate; 4 A molecular sieve; water; piperdinium acetate; diisobutylaluminium hydride; potassium carbonate; acetic acid; 4-methylmorpholine N-oxide; sodium sulfate; trifluoroacetic acid; zinc; In methanol; ethanol; dichloromethane; water; ethyl acetate; toluene; tert-butyl alcohol;

Reference yield:

: 880152-29-4
4-[2-(2-ethoxycarbonyl-cyclohex-1-enyl)-ethyl]-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

: 880152-39-6
C₃₆H₄₅NO₄Si

Guidance literature:: Multi-step reaction with 12 steps

1: pyridinium p-toluenesulfonate / methanol / 1 h / Heating

2: imidazole / CH₂Cl₂ / 20 °C

3: 12.0 g / DIBAL-H / CH₂Cl₂ / -78 - 0 °C

4: pyridine / 20 °C

5: 100 percent / TFA / CH₂Cl₂ / 1 h / 0 °C

6: 61 percent / pyridine / ethanol / 48 h / Heating

7: K₂CO₃ / methanol; H₂O / 1 h / 20 °C

8: 504.0 mg / N-methylmorpholine-N-oxide; TPAP; 4 Angstroem molecular sieves / CH₂Cl₂ / 1 h / 20 °C

9: 68 percent / Na₂SO₄; piperidinium acetate / ethyl acetate; toluene / Heating

10: 76 percent / N-chlorosuccinimide; H₂O / 2-methyl-propan-2-ol / 1 h / 20 °C

11: 66 percent / N-methylmorpholine-N-oxide; TPAP; 4 Angstroem molecular sieves / CH₂Cl₂ / 4 h / 20 °C

12: 98 percent / Zn; HOAc / 2 h / 20 °C

With pyridine; 1H-imidazole; N-chloro-succinimide; tetrapropylammonium perruthennate; 4 A molecular sieve; water; pyridinium p-toluenesulfonate; piperdinium acetate; diisobutylaluminium hydride; potassium carbonate; acetic acid; 4-methylmorpholine N-oxide; sodium sulfate; trifluoroacetic acid; zinc; In methanol; ethanol; dichloromethane; water; ethyl acetate; toluene; tert-butyl alcohol;