3-Chloro-2-methylbenzoyl chloride

Base Information

Chemical Name:3-Chloro-2-methylbenzoyl chloride
CAS No.:21900-47-0
Molecular Formula:C₈H₆Cl₂O
Molecular Weight:189.041
Hs Code.:
DSSTox Substance ID:DTXSID30598425
Wikidata:Q82494182

Synonyms:3-Chloro-2-methylbenzoyl chloride;21900-47-0;SCHEMBL108670;3-chloro-methyl benzoyl chloride;DTXSID30598425;MTTVMWJGVXXDFM-UHFFFAOYSA-N;AKOS006308727;3-chloro-2-methylbenzoic acid chloride;DB-105449

Suppliers and Price of 3-Chloro-2-methylbenzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3-Chloro-2-methylbenzoyl chloride

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:187.9795702
Heavy Atom Count:11
Complexity:158

Purity/Quality:: 95%+ or 98%+ ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C=CC=C1Cl)C(=O)Cl

Technology Process of 3-Chloro-2-methylbenzoyl chloride

There total 4 articles about 3-Chloro-2-methylbenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7499-08-3
3-chloro-2-methylbenzoic acid

: 21900-47-0
3-chloro-2-methylbenzoic acid chloride

Guidance literature:: With thionyl chloride;

Reference yield:

: 54454-12-5
(3-chloro-2-methylphenyl)carbonitrile

: 21900-47-0
3-chloro-2-methylbenzoic acid chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent H₂SO₄ / 70 °C

2: sodium peroxide / H₂O / 1 h / 20 °C

3: SOCl₂ / 12 h / Heating

With thionyl chloride; sodium peroxide; sulfuric acid; In water; 1: Oxidation / 2: Oxidation / 3: Chlorination;
DOI:10.1002/ps.2780410210

Reference yield:

: 87-60-5
3-chloro-2-methylbenzenamine

: 21900-47-0
3-chloro-2-methylbenzoic acid chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaNO₂; aq. HCl

1.2: 37.9 percent / copper(I) cyanide / H₂O / 0.33 h / 20 °C

2.1: 70 percent H₂SO₄ / 70 °C

3.1: sodium peroxide / H₂O / 1 h / 20 °C

4.1: SOCl₂ / 12 h / Heating

With hydrogenchloride; thionyl chloride; sodium peroxide; sulfuric acid; sodium nitrite; In water; 1.1: Diazotization / 1.2: Substitution / 2.1: Oxidation / 3.1: Oxidation / 4.1: Chlorination;
DOI:10.1002/ps.2780410210