(C(CH₃)3C₆H₄OC₃H₆)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3⁽¹⁺⁾*Br^(1-)=(C(CH₃)3C₆H₄OC₃H₆)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3Br

Base Information

• Chemical Name: (C(CH₃)3C₆H₄OC₃H₆)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3⁽¹⁺⁾*Br^(1-)=(C(CH₃)3C₆H₄OC₃H₆)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3Br
• CAS No.: 1237133-02-6
• Molecular Formula: Br*C₇₅H₁₁₄NO₅
• Molecular Weight: 1189.64

Synonyms:(C(CH₃)3C₆H₄OC₃H₆)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3⁽¹⁺⁾*Br^(1-)=(C(CH₃)3C₆H₄OC₃H₆)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3Br

Chemical Property of (C(CH₃)3C₆H₄OC₃H₆)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3⁽¹⁺⁾*Br^(1-)=(C(CH₃)3C₆H₄OC₃H₆)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3Br

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Technology Process of (C(CH₃)3C₆H₄OC₃H₆)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3⁽¹⁺⁾*Br^(1-)=(C(CH₃)3C₆H₄OC₃H₆)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3Br

There total 7 articles about (C(CH₃)3C₆H₄OC₃H₆)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3⁽¹⁺⁾*Br^(1-)=(C(CH₃)3C₆H₄OC₃H₆)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

tri-n-hexylamine (102-86-3) + C57H75BrO5 (1237132-99-8) → (C(CH3)3C6H4OC3H6)3CC6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=(C(CH3)3C6H4OC3H6)3CC6H4OC4H8OCH2C6H4N(C6H13)3Br (1237133-02-6)

Guidance literature:

In acetonitrile; at 80 ℃; for 16h;

DOI:10.1002/ejic.200901141

Reference yield:

C57H76O6 (1237132-97-6) → (C(CH3)3C6H4OC3H6)3CC6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=(C(CH3)3C6H4OC3H6)3CC6H4OC4H8OCH2C6H4N(C6H13)3Br (1237133-02-6)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus tribromide / toluene / 4 h / 0 - 20 °C

2: acetonitrile / 16 h / 80 °C

With phosphorus tribromide; In toluene; acetonitrile;

DOI:10.1002/ejic.200901141

Reference yield:

C11H15IO2 (1237132-95-4) → (C(CH3)3C6H4OC3H6)3CC6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=(C(CH3)3C6H4OC3H6)3CC6H4OC4H8OCH2C6H4N(C6H13)3Br (1237133-02-6)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 48 h / 20 °C

2: phosphorus tribromide / toluene / 4 h / 0 - 20 °C

3: acetonitrile / 16 h / 80 °C

With phosphorus tribromide; potassium carbonate; In N,N-dimethyl-formamide; toluene; acetonitrile;

DOI:10.1002/ejic.200901141

upstream raw materials:

C₅₇H₇₆O₆

tri-n-hexylamine

C₅₇H₇₅BrO₅

[4-(4-chlorobutoxy)phenyl]methanol

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